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Water-Cooled Condenser: Liebig's Glass Tube Corked in a Metal Pipe (Fownes, 1847)
Liebig's condenser as Fownes described it in 1847: a glass tube, tapering from end to end, held by bored corks in the centre of a metal pipe, with tubes that let a current of cold water run through the pipe around it. Vapour from a retort passes down the glass tube, condenses and runs into the receiver.
With a few pieces of ice in the little cistern the water stays at 32 °F (0 °C), and even very volatile liquids condense.
Unknown: the metal of the pipe, the material of the water tubes and all sizes. Fownes does not give them.
Source: G. Fownes, Elementary Chemistry (1847), p. 46 and Fig. 33. Picture: Fig. 33.
中级
Unknown
说明
1
1
Cork the glass tube into the pipe
Cork the glass tube into the pipe
Bore a cork for each end of the metal pipe. Pass the glass tube, which tapers from end to end, through both corks so that it is held in the centre of the pipe. Ours: the cork borer.
此步骤所需材料:
玻璃管1 tapering from end to end
未知金属1 the pipe
软木塞2 perforated
未知尺寸1 个所需工具:
软木塞打孔器2
2
Fit the water tubes
Fit the water tubes
Provide the pipe with tubes so arranged that a current of cold water can circulate through it. As drawn in Fig. 33, the water comes from a little cistern with a cock, standing above the apparatus, down to the lower end of the pipe, and leaves at the upper end into a jar.
此步骤所需材料:
未知材料1 water tubes and cistern所需工具:
软木塞打孔器3
3
Run the cold water
Run the cold water
While distilling, let cold water flow from the cistern through the pipe. For very volatile liquids put a few pieces of ice into the cistern: the water then stays at 32 °F (0 °C).
所需工具:
水
碎冰材料
5- 1 tapering from end to end占位符
- 1 the pipe占位符
- 2 perforated占位符
- 1 个占位符
- 1 water tubes and cistern占位符
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