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Zinc Sulphide Phosphor: Precipitated Sulphide Heated to Redness with a Flux (Thorpe 1913)
Charlie

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Charlie

28. 十月 2026DE
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Zinc Sulphide Phosphor: Precipitated Sulphide Heated to Redness with a Flux (Thorpe 1913)

Precipitated zinc sulphide does not glow. Heated to redness together with an alkali chloride or the sulphide of another metal, it turns into the phosphorescent sulphide used for fluorescent screens. Source: Thorpe, Dictionary of Applied Chemistry vol. 5 (1913), Zinc. Unknown: which chloride or sulphide, how much, and for how long. Thorpe names only the class, so the additive is linked to an unknown head. Crucible and furnace are ours. Picture drawn by Youblob.
中级
1 day

说明

1

Mix the sulphide with the additive

Grind precipitated zinc sulphide together with an alkali chloride or the sulphide of another metal. Unknown: which one and how much. Thorpe names only the class.

此步骤所需材料:

硫化锌硫化锌1 as required
未知助熔剂未知助熔剂1 as required

所需工具:

研钵与研杵研钵与研杵
2

Heat to redness

Heat the mixture to redness (ours: in a lidded porcelain crucible in a muffle furnace). Unknown: for how long. Let it cool.

所需工具:

带盖坩埚(瓷质)带盖坩埚(瓷质)
马弗炉马弗炉
坩埚钳坩埚钳
耐热手套耐热手套
3

Check the glow

Grind the cooled cake gently. Expose a little to light, then look at it in the dark: the phosphorescent sulphide glows.

所需工具:

研钵与研杵研钵与研杵

材料

2

所需工具

5

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