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Subcarbonate of Iron: Iron Sulfate and Soda Crystals, USP 1860
Youblob · CC0
Charlie

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Charlie

26. 十月 2026DE
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Subcarbonate of Iron: Iron Sulfate and Soda Crystals, USP 1860

Mix a solution of iron sulfate with one of washing soda and a reddish-brown powder settles out: the "precipitated carbonate of iron" of the 1860 US Pharmacopoeia. Washed and dried without heat, it is the starting point for reduced iron. Source: United States Pharmacopoeia, 4th decennial revision (1860, publ. 1863), Ferri Subcarbonas. The metric figures are our conversions. Picture drawn by Youblob.
初学者
2 days

说明

1

Dissolve the two salts

Dissolve 8 troy ounces (249 g) of iron sulfate in 4 pints (1.9 L) of water. Separately, dissolve 9 troy ounces (280 g) of carbonate of soda crystals in another 4 pints.

此步骤所需材料:

硫酸亚铁硫酸亚铁249 克
洗涤碱洗涤碱280 克
水水3.8 升

所需工具:

等臂天平等臂天平
玻璃器皿玻璃器皿
玻璃搅拌棒玻璃搅拌棒
2

Mix and let it settle

Pour the two solutions together, stir, and set it aside until the precipitate has settled.

所需工具:

玻璃器皿玻璃器皿
玻璃搅拌棒玻璃搅拌棒
3

Wash

Pour off the clear liquid. Wash the precipitate with water, settling and pouring off each time, until the washings pass nearly tasteless.

此步骤所需材料:

水水1 as required

所需工具:

玻璃器皿玻璃器皿
玻璃搅拌棒玻璃搅拌棒
4

Dry without heat

Dry it on blotting paper without heat. The result is a reddish-brown powder that dissolves in dilute hydrochloric acid with slight effervescence.

所需工具:

白色吸墨纸白色吸墨纸

材料

3
  • 占位符
  • 280 克
    占位符
  • 1 as required
    占位符

所需工具

4

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