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Ferrite Toroid Core: Copper-Zinc Ferrite Sintered at 1250 °C, Presintered Three Times at 900 °C (Snoek 1948, Ex. I)
A soft ferrite ring core for coils and transformers: copper, zinc and iron oxides with a little brownstone, presintered three times at 900 °C, pressed into a ring and sintered at 1250 °C in oxygen. Snoek's ring had an initial permeability of 1,580. Its Curie point was about 80 °C.
Source: J. L. Snoek, US 2,452,530 (Philips, 1948), Example I and its table. Unknown: the 'violet' iron oxide, linked to an unknown head. Picture: the patent's Fig. 4, the ring core.
Lanjutan
2 days
Instruksi
1
1
Weigh 20 : 30 : 50 mol % and 1 % brownstone
Weigh 20 : 30 : 50 mol % and 1 % brownstone
Mix 20 mol % pure copper oxide, 30 mol % pure zinc oxide and 50 mol % pure violet iron oxide, and add 1 % by weight of brownstone (manganese dioxide). Ours, by weight: 13.24 g copper oxide, 20.32 g zinc oxide and 66.44 g iron oxide per 100 g, plus 1 g brownstone. Unknown: what makes the iron oxide 'violet'; Snoek does not say.
Material untuk langkah ini:
Tembaga Oksida13.24 g
Serbuk Seng Oksida20.32 g
Oksida besi ungu66.44 g
Mangan dioksida (pirolusit)1 gAlat yang dibutuhkan:
Neraca lengan
Masker Debu2
2
Grind half an hour in an iron ball mill
Grind half an hour in an iron ball mill
Grind the mixture for half an hour in a mill with iron balls.
Alat yang dibutuhkan:
Ball Mill BesiMasker Debu3
3
Presinter at 900 °C for 2 hours in oxygen
Presinter at 900 °C for 2 hours in oxygen
Heat the ground powder to 900 °C for 2 hours in oxygen and let it cool.
Alat yang dibutuhkan:
Tungku Tabung
Oksigen
Tabung gas bertekanan
Pirometer
Krus dengan tutup (porselen)
Sarung Tangan Tahan Panas4
4
Grind and presinter at 900 °C again (2 of 3)
Grind and presinter at 900 °C again (2 of 3)
Grind the powder, then heat it once more to 900 °C in oxygen. Snoek gives no times for the repeats.
Alat yang dibutuhkan:
Ball Mill BesiTungku TabungOksigenTabung gas bertekananKrus dengan tutup (porselen)Sarung Tangan Tahan PanasMasker Debu5
5
Grind and presinter at 900 °C again (3 of 3)
Grind and presinter at 900 °C again (3 of 3)
Grind the powder, then heat it once more to 900 °C in oxygen. Snoek gives no times for the repeats.
Alat yang dibutuhkan:
Ball Mill BesiTungku TabungOksigenTabung gas bertekananKrus dengan tutup (porselen)Sarung Tangan Tahan PanasMasker Debu6
6
Grind 2 hours with iron balls
Grind 2 hours with iron balls
Grind it for 2 hours in a disintegrator with iron balls.
Alat yang dibutuhkan:
Ball Mill BesiMasker Debu7
7
Press a ring at 4 tons per cm²
Press a ring at 4 tons per cm²
Press the powder at 4 tons per square centimetre into a ring 3 cm across with a 4 × 4 mm cross-section.
Alat yang dibutuhkan:
Mesin pres hidrolik
Cetakan Penekan CincinMasker Debu8
8
Sinter at 1250 °C in oxygen, cool 5–10 °C a minute
Sinter at 1250 °C in oxygen, cool 5–10 °C a minute
Sinter the ring at 1250 °C in a current of oxygen. Example I heats for 1 hour and cools in the oxygen at 5 to 10 °C per minute. Snoek's ring had an initial permeability of 1,580, measured at room temperature at 2 kHz.
Alat yang dibutuhkan:
Tungku TabungOksigenTabung gas bertekananPirometer
Penjepit KowiSarung Tangan Tahan PanasBahan
4- 13.24 gPlaceholder
- 20.32 gPlaceholder
- 66.44 gPlaceholder
- Placeholder
Alat yang Diperlukan
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