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Magnesia Crucible: Strongly Calcined Magnesia Bound with Raw Magnesia and Baked at a Red Heat (Thorpe 1912)
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4. nóvember 2026NO
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Magnesia Crucible: Strongly Calcined Magnesia Bound with Raw Magnesia and Baked at a Red Heat (Thorpe 1912)

A magnesia crucible is a pot of magnesia, a basic refractory. Thorpe's Dictionary of Applied Chemistry (1912) gives the recipe introduced by Caron: magnesia shrinks a great deal when heated, so it is first calcined hotter than it will ever be used, then bound with 15-30 per cent of raw, slightly calcined magnesia and 10-15 per cent of water, moulded, dried and baked at a red heat. He gives no calcining temperature, mould or size; those are unknown here. Source: Thorpe, Dictionary of Applied Chemistry vol. II (1912), CRUCIBLES, p. 170. Picture: that passage.
Miðlungs
Two to three days

Leiðbeiningar

1

Read Thorpe

"The highly heated magnesia would not cohere without admixture with the raw material."
2

Calcine most of the magnesia hard

Magnesia contracts considerably when heated, so before making it into a crucible expose it to a higher temperature than the crucible will meet in use. The temperature itself is not given. Keep back a part of the magnesia only slightly calcined.

Efni fyrir þetta skref:

MagnesíumoxíðMagnesíumoxíð1 as required

Nauðsynleg verkfæri:

BrennsluofnBrennsluofn
Hitaþolnir hanskarHitaþolnir hanskar
3

Make the paste

Grind the strongly calcined magnesia and mix it with 15-30 per cent of the raw (slightly calcined) magnesia and 10-15 per cent of water into a paste. The raw part is what makes it hold together.

Efni fyrir þetta skref:

VatnVatn1 10-15 per cent

Nauðsynleg verkfæri:

Mortél og stauturMortél og stautur
Nákvæm stafræn vogNákvæm stafræn vog
RykgrímaRykgríma
4

Mould the crucible

Mould the paste into crucibles. Thorpe does not describe the mould or give sizes (unknown).

Nauðsynleg verkfæri:

Óþekktur efniviðurÓþekktur efniviður
Óþekkt málÓþekkt mál
5

Dry and bake

Dry the crucibles, then bake them at a red heat. Thorpe notes that magnesia crucibles are not harmed by standing in the air.

Nauðsynleg verkfæri:

BrennsluofnBrennsluofn
Hitaþolnir hanskarHitaþolnir hanskar
6

History and honest limits

Thorpe credits Caron with introducing magnesia for crucibles and for lining reverberatory furnaces in which steel was melted and dephosphorised. He also lists magnesia-bauxite crucibles (Gaudin) and calcined magnesite with a boron compound (Rawson and Littlefield, 1900). The calcining temperature, the mould, the size and the drying are not given; the tools are ours.

Efni

2
  • 1 as required
    Staðgengill
  • 1 10-15 per cent
    Staðgengill

Nauðsynleg verkfæri

7

CC0 opinbert ríki

Þessi teikning er gefin út undir CC0. Þér er frjálst að afrita, breyta, dreifa og nota þetta verk í hvaða tilgangi sem er, án þess að biðja um leyfi.

Studdu smiðinn með því að kaupa vörur í gegnum teikningu hans þar sem hann fær þóknun smiða sem seljendur ákvarða, eða búðu til nýja endurskoðun á þessari teikningu og tengdu hana sem tengingu í þinni eigin teikningu til að deila tekjum.

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