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Sodium Hydroxide Solution: Normal Caustic Soda, 40 g per Litre (Sutton, 1904)
The standard normal (1 M) caustic soda solution for titration: 40 g NaOH in each litre. Make it a little too strong, check it against normal acid, bring it to exact strength and keep it away from the air, which it takes carbon dioxide from.
Result: normal sodium hydroxide solution, its strength proved by titration.
Source: F. Sutton, A Systematic Handbook of Volumetric Analysis (1904), p. 48. Picture: that page of the book.
Byrjandi
Unknown
Leiðbeiningar
1
1
Dissolve the caustic soda
Dissolve the caustic soda
Dissolve pure caustic soda in distilled water until the solution has a specific gravity of about 1.05, about 50 g to the litre: a little stronger than normal (40 g to the litre). Expose it to the air as little as possible.
Efni fyrir þetta skref:
Natríumhýdroxíð — rannsóknarstofugæði1 about 50 g per litre
Eimað vatn1 solventNauðsynleg verkfæri:
Mæliglas2
2
Titrate and adjust
Titrate and adjust
Estimate its strength roughly with normal acid and methyl orange. Then titrate 50 ml of it exactly against normal acid and adjust it to exact normal strength. Methyl orange works cold even if the solution has taken up some carbon dioxide; with litmus or phenolphthalein, titrate boiling. Not given: the dilution, implied by the adjustment. Ours: hydrochloric acid as the normal acid; methyl orange as the pH indicator solution.
Nauðsynleg verkfæri:
Saltsýra
pH-vísislausn
Búretta (gler)
Pípetta3
3
Store it
Store it
Once its strength is settled, keep it in a bottle that shuts out the air, or in full bottles with their glass stoppers lightly greased with vaseline.
Nauðsynleg verkfæri:
Glerflaska (glær)
VaselínEfni
2- 1 about 50 g per litreStaðgengill
- 1 solventStaðgengill
Efni úr tengdum teikningum
Þessi teikning býr til
CC0 opinbert ríki
Þessi teikning er gefin út undir CC0. Þér er frjálst að afrita, breyta, dreifa og nota þetta verk í hvaða tilgangi sem er, án þess að biðja um leyfi.
Studdu smiðinn með því að kaupa vörur í gegnum teikningu hans þar sem hann fær þóknun smiða sem seljendur ákvarða, eða búðu til nýja endurskoðun á þessari teikningu og tengdu hana sem tengingu í þinni eigin teikningu til að deila tekjum.


