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Barium Ferrite Disc Magnet: 1 mol BaCO3 to 3.5 mol Iron Oxide, 1330 °C (Went, Philips 1956, Ex. 3)
A barium ferrite with more iron oxide: 1 mol barium carbonate to 3.5 mol, made as in Example 1 and passed through a 1330 °C furnace in 20 minutes. Went's rod held 1,600 gauss with a coercive force of 1,990 oersted.
Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 3. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Juu
2 days
Maagizo
1
1
Weigh barium carbonate and iron oxide
Weigh barium carbonate and iron oxide
Weigh 201.1 g barium carbonate (1 mol) and 560.7 g ferric oxide (3.5 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.
Vifaa kwa hatua hii:
Kabonati ya bariamu (witherite)201.1 g
Oksidi ya feri560.7 gZana zinazohitajika:
Mizani ya mizani-mbili
Glavu za mpira
Kinga ya Kupumua ya P1002
2
Mill with alcohol 13.5 hours, dry and sieve
Mill with alcohol 13.5 hours, dry and sieve
Grind the mixture with alcohol in a ball mill for 13.5 hours, then dry it and sieve it.
Zana zinazohitajika:
Kinu cha mipira ya chuma
Etanoli ya maabara, 95 %
Tanuri la kukaushia
Ungo3
3
Knead with a binder and form
Knead with a binder and form
Mix 300 g of the powder with a binder such as polyvinyl alcohol (Went names it or nitrocellulose) into a kneadable mass. The patent extrudes rods about 3 mm across; ours: press discs at 1.5 tonnes per cm², as in its other examples. Dry them in air for about 24 hours.
Zana zinazohitajika:
Unga wa polivinili alkoholi
Mashine ya kubana ya haidroliki
Kalibu ya kubana diski
Tanuri la kukaushia4
4
Pass through a 1330 °C zone in 20 minutes
Pass through a 1330 °C zone in 20 minutes
Sinter in air at 1330 °C by passing the pieces through a 10 cm hot zone at 5 mm per minute: 20 minutes in the heat.
Zana zinazohitajika:
Tanuru ya Mrija
Glavu Zinazostahimili Joto5
5
Magnetise the discs
Magnetise the discs
The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.
Zana zinazohitajika:
Sumaku ya umeme
DiraVifaa
2- Kishikilia Nafasi
- 560.7 gKishikilia Nafasi
Zana Zinazohitajika
14- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
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- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
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