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Ferric Oxide: Hydroxide Precipitated from Ferric Chloride with Ammonia, Then Heated
Ferric oxide, Fe2O3, made by way of the hydroxide as Thorpe's Dictionary (1912) gives it. Ferric chloride solution with excess ammonia throws down a bulky, brown, slimy hydroxide, which shrinks a great deal as it dries. Heated, it slowly gives up its water at 320 °C; taken to dull redness it suddenly contracts and glows, and is then much less soluble in acids.
The picture: our diagram.
Mwanzo
1 day
Maagizo
1
1
Precipitate with excess ammonia
Precipitate with excess ammonia
Add excess ammonia to ferric chloride solution: the hydroxide comes down as a bulky, brown, slimy precipitate. No amounts are given. Ours: stir in a beaker in a fume hood.
Vifaa kwa hatua hii:
Myeyusho wa kloridi ya feriki1 as requiredZana zinazohitajika:
Myeyusho wa amonia - asilimia 25-28
Bikari ya kioo
Kikorogo
Kabati la kutoa mvuke (lenye bomba)
Miwani ya kinga dhidi ya kemikali
Glavu za mpira2
2
Filter, wash and dry (ours)
Filter, wash and dry (ours)
Ours: filter off the precipitate, wash it with water and dry it; it shrinks a great deal as it dries.
Zana zinazohitajika:
Karatasi ya Kuchuja
Faneli ya Kioo Yenye Bomba
Chupa ya kuoshea ya maabara
Maji yaliyosafishwa kwa mvuke
Tanuri la kukaushia3
3
Heat to dull redness
Heat to dull redness
Heat the dry hydroxide: it gives up its water slowly at 320 °C. Taken on to dull redness, the anhydrous oxide suddenly contracts and glows brightly. Ours: a porcelain crucible in a muffle furnace.
Zana zinazohitajika:
Kikaango cha kuyeyushia chenye mfuniko (kaure)
Tanuri ya muffle
Koleo la kaure ya kuyeyushia
Glavu Zinazostahimili JotoVifaa
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