Ushirikiano
SANAA
UREMBO NA USTAWI
UJANJA
UTAMADUNI NA HISTORIA
BURUDANI
MAZINGIRA
CHAKULA NA VINYWAJI
UHANDISI WA KINYUME
SAYANSI
MICHEZO
TEKNOLOJIA
VAZI
Hafnium: Iodide Vapour Split on a Tungsten Wire Heated beyond 1600 °C (van Arkel and de Boer, US 1,671,213)
Hafnium will not come out of its chloride and hydrogen as clean metal. Van Arkel and de Boer instead let the vapour of hafnium iodide pass a white-hot wire in an evacuated vessel: the iodide splits and pure hafnium grows on the wire.
Result: hafnium metal deposited on the wire.
Source: A. E. van Arkel and J. H. de Boer, US 1,671,213 (1928). The wire runs white-hot; iodine vapour is released. Picture: the patent drawing.
Juu
1 day
Maagizo
1
1
Set up the vessel and wire
Set up the vessel and wire
Hang a wire, for example of tungsten, inside the vessel, fixed with small screws to two leading-in wires sealed through its narrowed top. A side tube goes to a pump. For the high temperatures the iodides need, the patent advises a vessel of suitable metal such as chrome iron rather than glass.
Zana zinazohitajika:
Chombo cha kioo
Waya wa tungsteni
Chanzo cha nishati ya mkondo wa moja kwa moja2
2
Pump out the air
Pump out the air
Put the hafnium iodide in the vessel and pump out the air and any other gas that would spoil the reaction.
Vifaa kwa hatua hii:
Iodidi ya hafni1 as requiredZana zinazohitajika:
Pampu ya utupu3
3
Evaporate the iodide
Evaporate the iodide
Heat the vessel until the iodide gives enough vapour. The patent gives 400-600 °C only for zirconium iodide; for hafnium iodide the temperature is not given. Ours: a furnace round the vessel.
Zana zinazohitajika:
Tanuru ya Mrija4
4
Deposit hafnium on the white-hot wire
Deposit hafnium on the white-hot wire
Pass a current through the wire to heat it beyond 1600 °C while the iodide vapour flows along it. The iodide splits and hafnium deposits on the wire. Do not overheat: the deposit can alloy with the wire.
Zana zinazohitajika:
Chanzo cha nishati ya mkondo wa moja kwa moja
Kipima joto kaliWaya wa tungsteniVifaa
1- 1 as requiredKishikilia Nafasi
Zana Zinazohitajika
6- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- 1 vendor sell this, none ship to you yetKishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
Mchoro huu unatengeneza
CC0 Umma Wote
Mchoro huu umetolewa chini ya CC0. Uko huru kunakili, kubadilisha, kusambaza, na kutumia kazi hii kwa madhumuni yoyote, bila kuomba ruhusa.
Saidia Mtengenezaji kwa kununua bidhaa kupitia Mchoro wao ambapo wanapata Kamisheni ya Mtengenezaji iliyowekwa na Wachuuzi, au unda marudio mapya ya Mchoro huu na uiunganishe kama kiungo katika Mchoro wako kuchangia mapato.