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Semi-Cured Phenolic Sheet: Paper Dipped in Phenol Resin and Part-Cured at 120-130 °C (Lucas, Western Electric, US 1,470,990)
Charlie

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Charlie

31. Oktoba 2026DE
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Semi-Cured Phenolic Sheet: Paper Dipped in Phenol Resin and Part-Cured at 120-130 °C (Lucas, Western Electric, US 1,470,990)

Paper soaked in phenol resin is dried, then cured only part of the way, so the resin is stiff but not yet hard. Lucas did this before the final hot press so the press would not squeeze the resin out of the fibres. Result: a dry, partly cured phenolic sheet that a later coat of phenolic resin can still bond into. Source: Lucas, US 1,470,990 (Western Electric, 1923). Stopping before his final hot press is ours. Not given: the solvent in his resin, paper grade, mercerising strengths. Picture drawn by Youblob.
Kati
1 hour

Maagizo

1

Dip the paper in phenol resin

Run the paper through a bath of phenol resin of specific gravity about 0.970: about 2 minutes for plain paper, 1 minute or less if mercerised first. Ours: Liquid Bakelite as the resin; Lucas does not say how it was thinned.

Vifaa kwa hatua hii:

KaratasiKaratasi1 as required
Bakelaiti ya kimiminika (bidhaa ya mgandamano wa fenoli na formaldehaidi)Bakelaiti ya kimiminika (bidhaa ya mgandamano wa fenoli na formaldehaidi)1 as required

Zana zinazohitajika:

Mstari wa kulowesha pre-pregMstari wa kulowesha pre-preg
Kipima-uzito wa majimajiKipima-uzito wa majimaji
2

Optional: mercerise the paper first

For faster, fuller soaking, first pass the paper through caustic soda, squeeze, wash in water, neutralise in an acid, wash again and dry. Strengths and the acid: not given.

Zana zinazohitajika:

Kaustiki soda (hidroksidi ya sodiamu)Kaustiki soda (hidroksidi ya sodiamu)
Mstari wa kulowesha pre-pregMstari wa kulowesha pre-preg
3

Dry at about 90 °C

Dry the soaked paper in an oven at about 90 °C, just long enough to dry it.

Zana zinazohitajika:

Tanuri la kukaushiaTanuri la kukaushia
4

Part-cure at 120-130 °C

Pass the dry paper through a curing oven at 120-130 °C for about 10 minutes (Lucas's description; his claim 4 says 125 °C for about 10 seconds). The resin sets as stiff as the fibres, but does not harden through.

Zana zinazohitajika:

Oveni ya kukomazaOveni ya kukomaza
5

Dip again for 10-15 seconds and dry

Dip the part-cured paper in phenol resin again for 10-15 seconds, then dry at about 90 °C until it can be wound on a reel. Stop here: the sheet is semi-cured. Lucas's next step, stacking and hot pressing, cures it fully.

Vifaa kwa hatua hii:

Bakelaiti ya kimiminika (bidhaa ya mgandamano wa fenoli na formaldehaidi)Bakelaiti ya kimiminika (bidhaa ya mgandamano wa fenoli na formaldehaidi)1 as required

Zana zinazohitajika:

Mstari wa kulowesha pre-pregMstari wa kulowesha pre-preg
Tanuri la kukaushiaTanuri la kukaushia

Vifaa

2

Zana Zinazohitajika

5

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Blueprint zinazohusiana

Blueprint hizi zinashiriki maarifa — mbinu, vifaa au kanuni

Liquid Bakelite: Phenol and Formalin Heated Together, the Oily Layer Kept (Baekeland 1909)
Hatari

Liquid Bakelite: Phenol and Formalin Heated Together, the Oily Layer Kept (Baekeland 1909)

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Viwandani

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