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Tannic Acid: Powdered Galls Extracted with Ether and Alcohol (75:25)
Pelouze's way of getting tannic acid from galls uses ether; Thorpe's Dictionary (1913) notes that a mixture of 75 % ether and 25 % alcohol can be used in its place. The extract separates into two layers, and the lower one, a strong tannic acid solution, dries to a porous mass. No amounts are given. Ether is very flammable: no flame, fume hood.
The picture: our diagram.
Kati
1 day
Maagizo
1
1
Powder the galls
Powder the galls
Grind oak galls finely. Ours: a mortar.
Vifaa kwa hatua hii:
Vinundu vya mwaloni1 as requiredZana zinazohitajika:
Kinu na mchi wa jiwe2
2
Extract with 75 % ether, 25 % alcohol
Extract with 75 % ether, 25 % alcohol
Mix 75 parts commercial ether with 25 parts alcohol and extract the powder with it. Ours: shake in a stoppered bottle in a fume hood, away from any flame.
Zana zinazohitajika:
Dietili etha
Etanoli ya maabara, 95 %
Silinda yenye vipimo
Chupa za kioo zenye vizibo
Kabati la kutoa mvuke (lenye bomba)
Miwani ya kinga dhidi ya kemikali
Glavu za mpira3
3
Keep the lower layer and evaporate it
Keep the lower layer and evaporate it
The extract separates into two layers: gallic acid, wax and resins in the upper, a strong tannic acid solution in the lower. Evaporate the lower layer to a porous mass. Ours: separatory funnel, evaporating dish on a water bath.
Zana zinazohitajika:
Funeli ya Kutenganisha
Sahani ya Kuvukizia
Bafu la Maji
Kabati la kutoa mvuke (lenye bomba)Vifaa
1- 1 as requiredKishikilia Nafasi
Zana Zinazohitajika
11- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
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