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Tin Oxide: Tin Burnt in an Open Iron Pot
Tin oxide is made by burning tin in air: melted tin in an open pot slowly turns to a white powder. Andrew Ure (1839) describes the enamel makers' way, with a lead-tin alloy in a flat iron pot, the powder raked aside as it forms, then ground and washed fine. Done with pure tin it gives the milky white oxide used in glazes, opal glass and polishing.
The picture: tin(IV) oxide powder on a watch glass.
Kati
A day
Maagizo
1
1
Melt the tin in an open pot
Melt the tin in an open pot
Melt the tin in a flat cast-iron pot over a charcoal fire. Leave the pot open to the air.
Vifaa kwa hatua hii:
Kipande cha bati (tin)1 kg
Mkaa1 as requiredZana zinazohitajika:
Mizani ya mizani-mbili
Chungu cha kuyeyushia cha chuma cha kutupwa
Tanuru la mkaa
Koleo
Glavu Zinazostahimili Joto2
2
Burn it, rake the powder aside
Burn it, rake the powder aside
Raise the heat towards a dull red and keep stirring the surface. Rake the white crust to the sides as it forms, as Ure describes, and add tin as it is used up. Keep the heat as low as will do: Ure warns that too strong a fire fuses the powder and makes it hard to grind.
Zana zinazohitajika:
Chungu cha kuyeyushia cha chuma cha kutupwa
Reki ya chuma
Kichota chenye matundu
Glavu Zinazostahimili Joto3
3
Pick out the metal
Pick out the metal
Let the powder cool. Sift it and pick out any beads of tin; Ure: no metal may be left in the oxide. Melt the beads back in.
Zana zinazohitajika:
Ungo Mwembamba
Miwani ya kinga dhidi ya kemikali4
4
Grind and wash
Grind and wash
Grind the powder fine with water. Stir it up in a bucket of water, let the coarse part settle for a moment and pour off the milky water; let the fine part settle out of that, as Ure washed his. Dry it in a dish and store it closed.
Vifaa kwa hatua hii:
Maji10 litaZana zinazohitajika:
Kinu na mchi
Kisagio cha mkono
Ndoo
Sahani ya Kuvukizia
Chupa ya Kioo5
5
Tin to oxide
Tin to oxide
Inapakia daftari la Jupyter…
6
6
Limits
Limits
Burning tin in air is how tin oxide is made (Wikipedia); the pot, raking, low heat and washing are Ure's practice for the lead-tin calx of enamel makers, used here with pure tin by our choice. Tin oxidises more slowly than Ure's lead-rich alloy, so allow time.
Vifaa
3- Kishikilia Nafasi
- 1 as requiredKishikilia Nafasi
- 10 litaKishikilia Nafasi
Zana Zinazohitajika
14- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
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- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
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Mchoro huu unatengeneza
CC0 Umma Wote
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Saidia Mtengenezaji kwa kununua bidhaa kupitia Mchoro wao ambapo wanapata Kamisheni ya Mtengenezaji iliyowekwa na Wachuuzi, au unda marudio mapya ya Mchoro huu na uiunganishe kama kiungo katika Mchoro wako kuchangia mapato.
