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Titanium: Titanium Tetrachloride Heated with Sodium in a Steel Bomb (Hunter, Thorpe 1913)
Sodium strips the chlorine from titanium tetrachloride inside a sealed steel bomb, leaving titanium metal in common salt.
Result: very pure titanium that looks like polished steel; hard and brittle cold, forgeable at low red heat, melting at 1800–1850 °C.
Source: Thorpe, Dictionary of Applied Chemistry vol. 5 (1913), p. 501, after Hunter (J. Amer. Chem. Soc. 1910, 32, 330). Unknown: how the titanium is freed from the salt; Thorpe does not give it. Picture drawn by Youblob.
Juu
1 day
Maagizo
1
1
Charge the steel bomb
Charge the steel bomb
Weigh pure titanium tetrachloride and about half its weight of sodium into a steel bomb, and close it.
Vifaa kwa hatua hii:
Tetrakloridi ya titani1 as requiredZana zinazohitajika:
Sodiamu
Mizani ya dijitali ya usahihi
Bomu la chuma2
2
Heat to low red heat
Heat to low red heat
Heat the bomb to a low red heat. Ours: a muffle furnace.
Zana zinazohitajika:
Tanuri ya muffle
Koleo la kaure ya kuyeyushia3
3
Free the titanium
Free the titanium
Unknown: how the titanium is separated from the salt in the bomb. Thorpe does not give it.
Zana zinazohitajika:
Usafishaji usiojulikanaVifaa
1- 1 as requiredKishikilia Nafasi
Zana Zinazohitajika
6- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
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