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Metal Oxide Varistor: Zinc Oxide with 1 % Bismuth Oxide, 1100 °C, 1.0 mm (Masuyama 1972)
A non-linear resistor: the current through it rises far faster than the voltage across it. Masuyama, Matsuoka and Nishi made one from zinc oxide with a little bismuth oxide: pressed into a disc, sintered, lapped, and given metal electrodes. With 1 mole % bismuth oxide, sintered at 1100 °C and lapped to 1.0 mm, the disc measured a C-value of 56 at 1 mA and a nonlinearity exponent n of 4.0.
Source: T. Masuyama, M. Matsuoka and T. Nishi (Matsushita), US 3,663,458 (1972), Example 1. Unknown: how the aluminium is sprayed on and what the silver paint is. The patent calls both well known, so they are linked to unknown heads. The 10 g batch is our arithmetic. Picture: the patent's drawing.
Juu
1 day
Maagizo
1
1
Weigh 99 : 1 and wet-mill 5 hours
Weigh 99 : 1 and wet-mill 5 hours
Mix zinc oxide and bismuth oxide 99 : 1 by moles. Ours, for 10 g: 9.453 g zinc oxide, 0.547 g bismuth oxide (our arithmetic). Mill wet for 5 hours, then dry. Unknown: the milling liquid.
Vifaa kwa hatua hii:
Poda ya oksidi ya zinki9.453 g
Oksidi ya bismuthi0.547 gZana zinazohitajika:
Mizani ya mizani-mbili
Kinu cha mipira ya chuma
Tanuri la kukaushia2
2
Press discs 13 mm by 2.5 mm
Press discs 13 mm by 2.5 mm
Press the powder in a mould into discs 13 mm across and 2.5 mm thick at 340 kg/cm².
Zana zinazohitajika:
Mashine ya kubana ya haidroliki
Kalibu ya kubana diski
Kalipa ya Vernier3
3
Sinter 1 hour at 1100 °C and furnace-cool
Sinter 1 hour at 1100 °C and furnace-cool
Sinter the discs in air for 1 hour at 1100 °C, then let them cool in the furnace to room temperature (about 15-30 °C).
Zana zinazohitajika:
Tanuri ya muffle4
4
Lap both faces to 1.0 mm
Lap both faces to 1.0 mm
Lap both faces with 600-mesh silicon carbide until the disc is 1.0 mm thick.
Zana zinazohitajika:
Kalipa ya Vernier5
5
Spray aluminium electrodes and attach leads
Spray aluminium electrodes and attach leads
Spray a metallised film of aluminium on both faces. Attach a lead wire to each with conductive silver paint. Unknown: the spraying method and the paint.
Vifaa kwa hatua hii:
Kitalu cha alumini1 as required
Rangi ya fedha inayopitisha umeme1 as required
Waya wa Shaba2 vipandeZana zinazohitajika:
Njia isiyojulikana ya kunyunyizia chuma
Kalipa ya VernierVifaa
5- 9.453 gKishikilia Nafasi
- 0.547 gKishikilia Nafasi
- 1 as requiredKishikilia Nafasi
- 1 as requiredKishikilia Nafasi
- 2 vipandeKishikilia Nafasi
Zana Zinazohitajika
9- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
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