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Metal Oxide Varistor: Zinc Oxide with Manganese and Chromic Oxides, Bismuth Paste Fired On (Masuyama 1972, Ex. 6)
A varistor with manganese dioxide and chromic oxide mixed into the zinc oxide, and bismuth oxide fired on from a paste: 99.0 % zinc oxide, 0.5 % manganese dioxide and 0.5 % chromic oxide by moles, sintered at 1350 °C, coated with bismuth oxide paste and fired at 800 °C. The disc measured a C-value of 282 at 1 mA and a nonlinearity exponent n of 25.6.
Source: T. Masuyama, M. Matsuoka and T. Nishi (Matsushita), US 3,663,458 (1972), Example 6. Unknown: how the aluminium is sprayed on, what the silver paint is, and how strong the epoxy solution of the paste is. The 10 g batch is our arithmetic. Picture: the patent's drawing.
Juu
2 days
Maagizo
1
1
Weigh 99 : 0.5 : 0.5 and wet-mill 5 hours
Weigh 99 : 0.5 : 0.5 and wet-mill 5 hours
Mix zinc oxide, manganese dioxide and chromic oxide 99 : 0.5 : 0.5 by moles. Ours, for 10 g: 9.854 g zinc oxide, 0.053 g manganese dioxide, 0.093 g chromic oxide (our arithmetic). Mill wet for 5 hours, then dry, as in Example 1. Unknown: the milling liquid.
Vifaa kwa hatua hii:
Poda ya oksidi ya zinki9.854 g
Dioksidi ya manganizi (pairolusiti)0.053 g
Oksidi ya Kromi0.093 gZana zinazohitajika:
Mizani ya mizani-mbili
Kinu cha mipira ya chuma
Tanuri la kukaushia2
2
Press discs 13 mm by 2.5 mm
Press discs 13 mm by 2.5 mm
Press discs 13 mm across and 2.5 mm thick at 340 kg/cm², as in Example 1.
Zana zinazohitajika:
Mashine ya kubana ya haidroliki
Kalibu ya kubana diski
Kalipa ya Vernier3
3
Sinter 1 hour at 1350 °C and furnace-cool
Sinter 1 hour at 1350 °C and furnace-cool
Sinter in air at 1350 °C for 1 hour and let the discs cool in the furnace.
Zana zinazohitajika:
Tanuri ya muffle4
4
Lap both faces
Lap both faces
Lap both faces with silicon carbide abrasive. Example 6 gives no thickness.
Zana zinazohitajika:
Kalipa ya Vernier5
5
Coat with bismuth oxide paste and fire at 800 °C
Coat with bismuth oxide paste and fire at 800 °C
Coat both lapped faces with a paste of 50 % by weight bismuth oxide in a solution of epoxy resin in butyl alcohol, and fire it in air at 800 °C for 30 minutes. The bismuth oxide diffuses into the zinc oxide. Not given: how much paste, or the strength of the epoxy solution.
Vifaa kwa hatua hii:
Oksidi ya bismuthi1 as requiredZana zinazohitajika:
Utomvu wa epoksi
n-Butanol
Tanuri ya muffle6
6
Spray aluminium electrodes and attach leads
Spray aluminium electrodes and attach leads
Spray a metallised film of aluminium on both faces. Attach a lead wire to each with conductive silver paint, as in Example 1. Unknown: the spraying method and the paint.
Vifaa kwa hatua hii:
Kitalu cha alumini1 as required
Rangi ya fedha inayopitisha umeme1 as required
Waya wa Shaba2 vipandeZana zinazohitajika:
Njia isiyojulikana ya kunyunyizia chuma
Kalipa ya VernierVifaa
7- 9.854 gKishikilia Nafasi
- Kishikilia Nafasi
- 0.093 gKishikilia Nafasi
- 1 as requiredKishikilia Nafasi
- 1 as requiredKishikilia Nafasi
- 1 as requiredKishikilia Nafasi
- 2 vipandeKishikilia Nafasi
Zana Zinazohitajika
11- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
- Kishikilia Nafasi
Mchoro huu unatengeneza
Blueprint zinazohusiana
Blueprint hizi zinashiriki maarifa — mbinu, vifaa au kanuni
CC0 Umma Wote
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