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Metal Oxide Varistor: Zinc Oxide with 0.5 % Barium Oxide, Bismuth-Manganese Oxide Paste Fired On (Masuyama 1972, Ex. 7)
A varistor whose bismuth oxide and manganese dioxide are both fired on from a paste: 99.5 % zinc oxide with 0.5 % barium oxide by moles, sintered at 1350 °C, coated with a 70 : 30 bismuth oxide and manganese dioxide paste and fired at 800 °C. The disc measured a C-value of 77 at 1 mA and a nonlinearity exponent n of 43.1.
Source: T. Masuyama, M. Matsuoka and T. Nishi (Matsushita), US 3,663,458 (1972), Example 7. Unknown: what the silver paint is, and how strong the epoxy solution of the paste is. The spraying is ours, after US Army Corps of Engineers EM 1110-2-3401 (1999). The 10 g batch is our arithmetic. Picture: the patent's drawing.
고급
2 days
안내
1
1
Weigh 99.5 : 0.5 and wet-mill 5 hours
Weigh 99.5 : 0.5 and wet-mill 5 hours
Mix zinc oxide and barium oxide 99.5 : 0.5 by moles. Ours, for 10 g: 9.906 g zinc oxide, 0.094 g barium oxide (our arithmetic). Mill wet for 5 hours, then dry, as in Example 1. Unknown: the milling liquid.
이 단계의 재료:
산화아연 분말9.906 g
산화바륨0.094 g필요한 도구:
접시 저울
철 볼 밀
건조 가마2
2
Press discs 13 mm by 2.5 mm
Press discs 13 mm by 2.5 mm
Press discs 13 mm across and 2.5 mm thick at 340 kg/cm², as in Example 1.
필요한 도구:
유압 프레스
원판 압축 금형
버니어 캘리퍼스3
3
Sinter 1 hour at 1350 °C and furnace-cool
Sinter 1 hour at 1350 °C and furnace-cool
Sinter in air at 1350 °C for 1 hour and let the discs cool in the furnace.
필요한 도구:
머플로4
4
Lap both faces
Lap both faces
Lap both faces with silicon carbide abrasive. Example 7 gives no thickness.
필요한 도구:
탄화규소 연마입자버니어 캘리퍼스5
5
Coat with bismuth and manganese oxide paste, fire at 800 °C
Coat with bismuth and manganese oxide paste, fire at 800 °C
Coat both lapped faces with a paste whose solids are 70 % bismuth oxide and 30 % manganese dioxide by weight, and fire it in air at 800 °C for 30 minutes. Example 7 does not name the paste's liquid; ours: the epoxy-resin butyl-alcohol solution of Example 4. Not given: how much paste.
이 단계의 재료:
산화 비스무트1 as required
이산화망가니즈 (연망가니즈석)1 as required필요한 도구:
에폭시 수지
n-뷰탄올머플로6
6
Spray aluminium electrodes and attach leads
Spray aluminium electrodes and attach leads
Spray a metallised film of aluminium on both faces. Attach a lead wire to each with conductive silver paint, as in Example 1. Ours, after US Army Corps of Engineers EM 1110-2-3401 (1999): wire-arc spray the aluminium from two 3.2 mm wires melted by an 18-40 V DC arc and atomised by compressed air, 15-20 cm from the disc and never at less than 45°, in at least two coats at right angles of 50-75 µm each. Unknown: the paint.
이 단계의 재료:
알루미늄 잉곳1 as 3.2 mm spray wire
은 도전성 도료1 as required
구리선2 개필요한 도구:
버니어 캘리퍼스
아크 용사 건
산업용 공기 압축기재료
7- 9.906 g플레이스홀더
- 0.094 g플레이스홀더
- 1 as required플레이스홀더
- 1 as required플레이스홀더
- 1 as 3.2 mm spray wire플레이스홀더
- 1 as required플레이스홀더
- 2 개플레이스홀더
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