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Ceramic Disc Capacitors: Barium Titanate with Nickel Stannate, Pressed, Fired and Silvered (Coffeen, US 2,789,061)
Ed

Dicipta oleh

Ed

2. November 2026FI
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Ceramic Disc Capacitors: Barium Titanate with Nickel Stannate, Pressed, Fired and Silvered (Coffeen, US 2,789,061)

Barium titanate with 3 mole % nickel stannate is calcined, pressed into small discs and fired hard. Silver is fired onto both faces and a lead soldered to each, giving ceramic disc capacitors of high capacity for their size. Result: discs 3/8 inch across and about 1/10 inch thick with a dielectric constant averaging 2380 and a dissipation factor of 0.58 %. Between 25 and 85 °C the dielectric constant rose at most 17 % and fell at most 7 %. Source: W. W. Coffeen (Metal & Thermit Corp.), US 2,789,061 (1957). Unknown: how the barium titanate, the nickel stannate and the tinned lead wire are made; the patent uses them ready-made. Picture: Wikimedia Commons.
Lanjutan
10 days

Arahan

1

Weigh and slurry

Weigh 19.32 g of barium titanate and 0.68 g of hydrated nickel stannate (about NiSnO3·2H2O), which is 97 mole % BaTiO3 and 3 mole % NiSnO3. Slurry them with 50 cc of distilled water. The patent prefers 2 to 4 mole % nickel stannate; 1 to 15 % works.

Bahan untuk langkah ini:

Barium titanatBarium titanat19.32 g
Nikel stanatNikel stanat0.68 g

Alatan diperlukan:

Air SulingAir Suling
Penimbang Digital JituPenimbang Digital Jitu
Piring PenyejatPiring Penyejat
2

Dry, sieve and calcine

Dry the slurry, crush it to pass a 50 mesh screen, moisten it with 5 % of a 2 1/2 % starch solution and press it into one slug. Calcine the slug for one hour at 1600 °F (871 °C). Ours: potato starch, a drying oven, mortar and pestle.

Alatan diperlukan:

Kanji kentangKanji kentang
Ketuhar pengeringanKetuhar pengeringan
Lesung dan AluLesung dan Alu
AyakAyak
Mesin tekan hidraulikMesin tekan hidraulik
Tanur suhu tinggiTanur suhu tinggi
3

Press the discs

Grind the calcine to pass a 325 mesh screen, moisten it again with starch solution, and press small discs 3/8 inch in diameter and about 1/10 inch thick at 20,000 pounds per square inch.

Alatan diperlukan:

Lesung dan AluLesung dan Alu
Ayak Bermata HalusAyak Bermata Halus
Kanji kentangKanji kentang
Mesin tekan hidraulikMesin tekan hidraulik
Acuan tekan cakeraAcuan tekan cakera
4

Fire on platinum

Fire the discs on platinum foil at 2400 °F (1316 °C) for one hour. They come out with zero absorption.

Alatan diperlukan:

Tanur suhu tinggiTanur suhu tinggi
PlatinumPlatinum
5

Silver and lead

Paint silver paint on both faces and fire the discs at 1350 °F (732 °C) for one hour. Solder tinned copper lead wires directly to the silver electrodes. Age at least a week before measuring. Ours: a fine brush and a soldering iron.

Bahan untuk langkah ini:

Cat perak bakarCat perak bakar1 both faces
Dawai kuprum bersalut timahDawai kuprum bersalut timah2 leads per disc
Dawai PateriDawai Pateri1 a little

Alatan diperlukan:

Berus berhujung halusBerus berhujung halus
Tanur suhu tinggiTanur suhu tinggi
Alat pematerianAlat pematerian

Bahan

5

Alatan Diperlukan

14

CC0 Domain Awam

Blueprint ini dikeluarkan di bawah CC0. Anda bebas menyalin, mengubah, mengedar, dan menggunakan karya ini untuk sebarang tujuan, tanpa meminta kebenaran.

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