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Fired Silver Paint: Precipitated Silver and Flux in Polyvinyl Alcohol with Ammonia (Gray, Erie Resistor 1954, Ex. 1)
Ed

Dicipta oleh

Ed

28. Oktober 2026FI
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Fired Silver Paint: Precipitated Silver and Flux in Polyvinyl Alcohol with Ammonia (Gray, Erie Resistor 1954, Ex. 1)

A paint for putting silver electrodes on ceramic, glass or mica. Fine silver powder and a little ceramic flux are held in polyvinyl alcohol dissolved in water, with a trace of ammonia to make the wet paint conduct. So a capacitor can be measured while it is being painted. On firing, the silver becomes a film held on by the flux. The silver settles, so stir while painting. Source: Robert B. Gray, US 2,695,275 (Erie Resistor, 1954), Example 1. Not given: how the silver was precipitated, which flux, the form of the ammonia, and the firing heat. Ours: precipitated silver made by reducing silver chloride with zinc, bismuth subnitrate as the flux (one Gray names), and strong ammonia water. Picture drawn by Youblob.
Pemula
1 day

Arahan

1

Dissolve 4 g polyvinyl alcohol in the water

For 100 g of paint: dissolve 4 g polyvinyl alcohol in the water, warming it to help it dissolve. The water is the balance, about 35 to 44 g. Warming is ours.

Bahan untuk langkah ini:

Serbuk polivinil alkoholSerbuk polivinil alkohol4 g
Air SulingAir Suling1 as required

Alatan diperlukan:

Neraca dua piringNeraca dua piring
Bikar BorosilikatBikar Borosilikat
Plat PemanasPlat Pemanas
Rod Kaca BorosilikatRod Kaca Borosilikat
2

Grind in 50 g precipitated silver and the flux

Grind 50 g precipitated silver and 2 to 10 g ceramic flux into the solution until smooth. Gray allows some silver chloride left in the silver. Ours: silver from the zinc route, and bismuth subnitrate, one of the fluxes Gray names. The right amount of flux depends on the ceramic.

Bahan untuk langkah ini:

Perak mendakanPerak mendakan50 g
Bismut subnitratBismut subnitrat1 as required

Alatan diperlukan:

Neraca dua piringNeraca dua piring
Lesung dan AluLesung dan Alu
Sarung Tangan NitrilSarung Tangan Nitril
3

Add 0.2 to 1 % ammonia

Stir in ammonia, 0.2 to 1 % of the paint. It evaporates from the film but makes the wet paint conduct. Ours: added as strong ammonia water. Sharp fumes: work in air, goggles.

Bahan untuk langkah ini:

Larutan ammonia 25-28 %Larutan ammonia 25-28 %1 as required

Alatan diperlukan:

Rod Kaca BorosilikatRod Kaca Borosilikat
Gogal Percikan KimiaGogal Percikan Kimia
Sarung Tangan NitrilSarung Tangan Nitril
4

Stir while painting

The silver in this paint settles, so stir it while it is being applied.

Alatan diperlukan:

Rod Kaca BorosilikatRod Kaca Borosilikat

Bahan

5

Alatan Diperlukan

7

CC0 Domain Awam

Blueprint ini dikeluarkan di bawah CC0. Anda bebas menyalin, mengubah, mengedar, dan menggunakan karya ini untuk sebarang tujuan, tanpa meminta kebenaran.

Sokong Pembuat dengan membeli produk melalui Blueprint mereka di mana mereka memperoleh Komisen Pembuat ditetapkan oleh Penjual, atau cipta iterasi baru Blueprint ini dan sertakan ia sebagai sambungan dalam Blueprint anda sendiri untuk berkongsi hasil.

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