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Neodymium Magnets, Sample 10: 68Fe-17B-15Nd Sintered (Sagawa 1988)
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28. Oktober 2026NO
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Neodymium Magnets, Sample 10: 68Fe-17B-15Nd Sintered (Sagawa 1988)

Neodymium magnets are iron, boron and neodymium. Sagawa's team at Sumitomo melted the three together, ground the casting to a powder finer than 10 µm, lined the grains up in a magnetic field while pressing them, and sintered the compact in argon. This is their sample 10, 68 % iron, 17 % boron and 15 % neodymium by atoms: 17.6 MGOe. Source: M. Sagawa et al. (Sumitomo Special Metals), US 4,770,723 (1988). Unknown: how the pure iron, the ferroboron and the neodymium metal are made; the patent does not say. The magnetising is ours, after Przybylski et al., Sensors 16:569 (2016). The 1 kg weights are our arithmetic from the patent's atomic percentages. Picture: the patent's Fig. 8.
Pakar
2 days

Arahan

1

Weigh sample 10: 68 Fe, 17 B, 15 Nd

Sample 10 is 68 % iron, 17 % boron and 15 % neodymium by atoms. Use 99.9 % electrolytic iron, ferroboron (19.38 % B, 5.32 % Al, 0.74 % Si, 0.03 % C, the rest iron) and neodymium of 99.7 % or better. Ours: a 1 kg melt, by arithmetic: 503.0 g iron, 154.3 g ferroboron, 352.1 g neodymium. Unknown: how these three are made.

Bahan untuk langkah ini:

Besi elektrolitikBesi elektrolitik503 g
FerroboronFerroboron154.3 g
Logam neodimiumLogam neodimium352.1 g

Alatan diperlukan:

Neraca dua piringNeraca dua piring
2

Melt by high frequency in argon and cast

Melt the charge in a high-frequency (induction) furnace under argon and pour it into a water-cooled copper mould.

Alatan diperlukan:

Relau aruhanRelau aruhan
Mangkuk Pijar Tanah Liat Tahan ApiMangkuk Pijar Tanah Liat Tahan Api
ArgonArgon
Silinder gas bertekananSilinder gas bertekanan
Acuan kuprum disejukkan airAcuan kuprum disejukkan air
Sarung Tangan Tahan HabaSarung Tangan Tahan Haba
3

Stamp to 35 mesh, ball-mill to 3-10 µm

Crush the casting in a stamp mill until it passes a 35-mesh sieve. Then grind it in a ball mill for 3 hours, to 3-10 µm.

Alatan diperlukan:

Kilang PenumbukKilang Penumbuk
Set penapis (mata bergred)Set penapis (mata bergred)
Kilang Bebola BesiKilang Bebola Besi
Cermin mata keselamatanCermin mata keselamatan
4

Press in a 10 kOe field at 1.5 t/cm²

Line the powder up in a magnetic field of 10 kOe and press it at 1.5 tonnes per cm². Unknown: the size and shape of the magnets.

Alatan diperlukan:

Penekan medan magnetPenekan medan magnet
5

Sinter in argon at 1000-1200 °C

Sinter the compacts at 1000-1200 °C for about one hour in argon, then let them cool. Sample 10 measured 8.7 kG remanence, 7.6 kOe coercivity and 17.6 MGOe.

Alatan diperlukan:

Relau TiubRelau Tiub
ArgonArgon
Silinder gas bertekananSilinder gas bertekanan
Sarung Tangan Tahan HabaSarung Tangan Tahan Haba
6

Magnetise the magnets

Ours, after Przybylski et al., Sensors 16:569 (2016): put each magnet in the coil of an impulse magnetiser and discharge a capacitor bank through it. They found a field of 1200 kA/m enough to saturate N38 sintered Nd-Fe-B; their magnetiser used a 1 mF bank charged up to 5000 V, a thyristor switch and a 440-turn coil of 3 mm copper wire with an 80 mm bore.

Alatan diperlukan:

PemagnetPemagnet

Bahan

3

Alatan Diperlukan

14

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