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Tannic Acid: Chinese Galls Extracted with Warm Water, Shaken with Ether and Dried on Tin Sheets
Charlie

Dicipta oleh

Charlie

21. Oktober 2026DE
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Tannic Acid: Chinese Galls Extracted with Warm Water, Shaken with Ether and Dried on Tin Sheets

This is the large-scale way to make commercial tannin, as Thorpe's Dictionary (1913) gives it. Chinese galls from sumach hold as much as 70 % tannin; the best oak galls, from Aleppo, 50–60 %. The powder is extracted with warm water, and the extract is shaken with ether. After several days the ether layer on top is taken off; the tannin stays in the lower layer, which is dried on hot tin sheets until it puffs up. The product still holds some gallic acid, wax and glucose. Ether is very flammable: no flame. The picture: our diagram.
Pertengahan
1 week

Arahan

1

Extract the powdered galls with warm water

Powder Chinese galls finely. Stir with enough water at 50–60 °C to make a strong extract. Filter it clear.

Bahan untuk langkah ini:

Gal CinaGal Cina1 as required

Alatan diperlukan:

AirAir
Lesung dan Alu BatuLesung dan Alu Batu
PengacauPengacau
Mandian AirMandian Air
Termometer MakmalTermometer Makmal
Kertas TurasKertas Turas
Corong Kaca BertangkaiCorong Kaca Bertangkai
2

Shake with a quarter volume of ether

Add ether, one quarter of the extract's volume, and agitate until it forms an emulsion. Let it stand for several days.

Alatan diperlukan:

Dietil EterDietil Eter
Corong pengasingCorong pengasing
Kabinet wasap (bersalur)Kabinet wasap (bersalur)
Gogal Percikan KimiaGogal Percikan Kimia
Sarung tangan getahSarung tangan getah
3

Take off the ether layer and recover the ether

Remove the upper ether layer. Run the lower layer, which holds all the tannin, into a still and distil off the ether in it to recover it. No flame near the ether.

Alatan diperlukan:

Corong pengasingCorong pengasing
Alembik tembagaAlembik tembaga
Kabinet wasap (bersalur)Kabinet wasap (bersalur)
4

Dry on tin sheets over a steam coil

Let the syrupy liquid cool, spread it on tin sheets and heat them with a steam coil. The tannin quickly puffs up and dries.

Alatan diperlukan:

Kepingan besi putihKepingan besi putih
Gegelung StimGegelung Stim
Dandang stimDandang stim
Sarung tangan getahSarung tangan getah

Bahan

1
  • 1 as required
    Pemegang Tempat

Alatan Diperlukan

16

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