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Bismuth Oxide: Subnitrate Boiled with Sodium Hydroxide Solution (British Pharmacopoeia, 1907)
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Bismuth Oxide: Subnitrate Boiled with Sodium Hydroxide Solution (British Pharmacopoeia, 1907)

Boil bismuth subnitrate with sodium hydroxide solution: bismuth hydroxide falls and sodium nitrate stays dissolved. At 100 °C the hydroxide loses its water, leaving bismuth oxide, a dull lemon-yellow powder. Source: The Dispensatory of the United States of America (1907), Bismuthi Oxidum, after the British Pharmacopoeia. Not given: amounts, strength or time; those are stated as not given. The 10 % lye, washing and filter are ours. Picture drawn by Youblob.
Àárín
half a day

Ìlànà

1

Boil the subnitrate with soda lye

Boil bismuth subnitrate with sodium hydroxide solution (ours: 10 %). Bismuth hydroxide is precipitated; sodium nitrate stays in solution. Not given: amounts and time. Goggles and gloves.

Àwọn ohun èlò fún ìgbésẹ̀ yìí:

Bismuth subnitrateBismuth subnitrate1 as required

Àwọn irinṣẹ́ tí a nílò:

Sodium hydroxide ní omi ìdá 10Sodium hydroxide ní omi ìdá 10
Ago BórósílíkéètìAgo Bórósílíkéètì
Pátákó GbígbónáPátákó Gbígbóná
Gílásì Ààbò Fún Ìfọ́n Kẹ́míkàGílásì Ààbò Fún Ìfọ́n Kẹ́míkà
Ìbọ̀wọ́ NítírílìÌbọ̀wọ́ Nítírílì
2

Wash and dry to the oxide

Filter off the precipitate and wash it (ours: with distilled water). Hold it at 100 °C: the hydroxide gives up its water and dull lemon-yellow bismuth oxide remains.

Àwọn irinṣẹ́ tí a nílò:

Bébà Ìsẹ́Bébà Ìsẹ́
Omi Àyọ́Omi Àyọ́
Ààrò ìgbẹ̀Ààrò ìgbẹ̀

Àwọn ohun-èlò

1

Àwọn irinṣẹ́ tó nílò

8

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