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Lactic Acid: Wackenroder's Calcium Lactate Split with Oxalic Acid (US Dispensatory 1907)
Wackenroder's lactic acid: skimmed milk, milk sugar, chalk and water kept warm for a month. As the acid forms, the chalk takes it up as calcium lactate. That salt is crystallised and then split with exactly enough oxalic acid to free the lactic acid; the lime falls as calcium oxalate.
Source: The Dispensatory of the United States of America (1907), Acidum Lacticum. Pharmacopoeial lactic acid, used as food-grade, as ruled. Unknown: how the free acid is separated afterwards; the Dispensatory does not say, so it is linked to an unknown head. The sulphuric-acid version is a separate blueprint. Picture drawn by Youblob.
Àárín
5 weeks
Ìlànà
1
1
Mix 10 : 2.5 : 2 : 20
Mix 10 : 2.5 : 2 : 20
Mix 10 parts skimmed milk, 2.5 parts milk sugar, 2 parts chalk and 20 parts water. Ours: grams.
Àwọn ohun èlò fún ìgbésẹ̀ yìí:
Wàrà tí a ti yọ ọ̀rá kúrò10 parts
Ṣúgà wàrà2.5 parts
Calcium carbonate (ẹfun funfun)2 parts
Omi20 partsÀwọn irinṣẹ́ tí a nílò:
Òǹwọ̀n ìdọ́gba
Ohun èlò dígí2
2
Digest at about 24 °C for a month
Digest at about 24 °C for a month
Keep it at about 23.8 °C (75 °F) for a month, or until the chalk has dissolved.
Àwọn irinṣẹ́ tí a nílò:
Ohun èlò dígí
Ẹ̀rọ Ìwọ̀n Ooru Yàrá Ìwádìí3
3
Press, clarify and crystallise the calcium lactate
Press, clarify and crystallise the calcium lactate
Press it out, clarify it, and evaporate it so the calcium lactate crystallises. Recrystallise it.
Àwọn irinṣẹ́ tí a nílò:
Aṣọ wàrà-dídì
Bébà Ìsẹ́
Àwo Ìgbẹ
Pátákó Gbígbóná4
4
Split the salt with oxalic acid
Split the salt with oxalic acid
Decompose the calcium lactate with oxalic acid in exactly the saturating proportion. Oxalic acid is poisonous if swallowed: gloves. Unknown: how the lactic acid is then separated.
Àwọn ohun èlò fún ìgbésẹ̀ yìí:
Acid oxalic dihydrate1 as requiredÀwọn irinṣẹ́ tí a nílò:
Ohun èlò dígí
Ìtọ́jú-ìkẹyìn tí a kò mọ̀
Gílásì Ààbò Fún Ìfọ́n Kẹ́míkà
Ìbọ̀wọ́ NítírílìÀwọn ohun-èlò
5- 10 partsÀyè
- 2.5 partsÀyè
- Àyè
- 20 partsÀyè
- 1 as requiredÀyè
Àwọn irinṣẹ́ tó nílò
10- Àyè
- Àyè
Ìtọ́nisọ́nà yìí ń ṣe
Blueprint tó jọra
Àwọn blueprint wọ̀nyí pín ìmọ̀ — ọ̀nà, ohun-èlò tàbí ìlànà
CC0 Àgbègbè Gbogbogbò
Blueprint yìí ti jáde lábẹ́ CC0. O lè ṣe àdàkọ, yí padà, pín, àti lò láìsí ìyọ̀ǹda.
Ṣàtìlẹ́yìn Olùṣẹ́dá nípa rírà àwọn ọjà nipasẹ̀ Blueprint wọn Ẹ̀san Olùṣẹ́dá tí àwọn Olùtajà gbé kalẹ̀, tàbí ṣẹ̀dá àtúnṣe tuntun ti Blueprint yìí kí o sì fi sínú Blueprint rẹ gẹ́gẹ́ bí ìsopọ̀ láti pín owó-wíwọlé.


