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Tannic Acid: Chinese Galls Extracted with Warm Water, Shaken with Ether and Dried on Tin Sheets
This is the large-scale way to make commercial tannin, as Thorpe's Dictionary (1913) gives it. Chinese galls from sumach hold as much as 70 % tannin; the best oak galls, from Aleppo, 50–60 %. The powder is extracted with warm water, and the extract is shaken with ether. After several days the ether layer on top is taken off; the tannin stays in the lower layer, which is dried on hot tin sheets until it puffs up. The product still holds some gallic acid, wax and glucose. Ether is very flammable: no flame.
The picture: our diagram.
Àárín
1 week
Ìlànà
1
1
Extract the powdered galls with warm water
Extract the powdered galls with warm water
Powder Chinese galls finely. Stir with enough water at 50–60 °C to make a strong extract. Filter it clear.
Àwọn ohun èlò fún ìgbésẹ̀ yìí:
Gálì Ṣáínà1 as requiredÀwọn irinṣẹ́ tí a nílò:
Omi
Odó àti Ọmọ Odó Òkúta
Ohun ìrúwé
Ìwẹ̀ Omi
Ẹ̀rọ Ìwọ̀n Ooru Yàrá Ìwádìí
Bébà Ìsẹ́
Kọ́nfù Gílásì Onípọ̀n2
2
Shake with a quarter volume of ether
Shake with a quarter volume of ether
Add ether, one quarter of the extract's volume, and agitate until it forms an emulsion. Let it stand for several days.
Àwọn irinṣẹ́ tí a nílò:
Diethyl ether
Fọ́nẹ́ẹ̀lì Ìyàpa
Àpótí eérú (tí ó ní ọ̀pá ìjáde)
Gílásì Ààbò Fún Ìfọ́n Kẹ́míkà
Ìbọ̀wọ́ rọ́bà3
3
Take off the ether layer and recover the ether
Take off the ether layer and recover the ether
Remove the upper ether layer. Run the lower layer, which holds all the tannin, into a still and distil off the ether in it to recover it. No flame near the ether.
Àwọn irinṣẹ́ tí a nílò:
Fọ́nẹ́ẹ̀lì Ìyàpa
Alembiki bàbà
Àpótí eérú (tí ó ní ọ̀pá ìjáde)4
4
Dry on tin sheets over a steam coil
Dry on tin sheets over a steam coil
Let the syrupy liquid cool, spread it on tin sheets and heat them with a steam coil. The tannin quickly puffs up and dries.
Àwọn irinṣẹ́ tí a nílò:
Pátákó irin funfun
Kọ́ìlì Ategun
Bọ́ìlà èéfín omi
Ìbọ̀wọ́ rọ́bàÀwọn ohun-èlò
1- 1 as requiredÀyè
Àwọn irinṣẹ́ tó nílò
16- Àyè
- Àyè
- Àyè
- Àyè
Ìtọ́nisọ́nà yìí ń ṣe
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