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Tannic Acid: Galls Stirred to a Cream with Ether and Pressed (Leconnet)
Leconnet's method (Annalen, 1836), as Thorpe's Dictionary (1913) gives it: stir powdered galls into ether until a thin cream forms, press it, and repeat until no more tannin comes out. Thorpe does not say how the pressed liquid is worked up; evaporating it is ours. Ether is very flammable: no flame, fume hood.
The picture: our diagram.
Àárín
1 day
Ìlànà
1
1
Stir powdered galls into ether to a thin cream
Stir powdered galls into ether to a thin cream
Grind oak galls finely and stir the powder into ether until the mixture is a thin cream. Ours: a mortar, then a stirrer in a fume hood, no flame.
Àwọn ohun èlò fún ìgbésẹ̀ yìí:
Èso ìdìlé igi oaku1 as requiredÀwọn irinṣẹ́ tí a nílò:
Diethyl ether
Odó àti Ọmọ Odó Òkúta
Ohun ìrúwé
Àpótí eérú (tí ó ní ọ̀pá ìjáde)
Gílásì Ààbò Fún Ìfọ́n Kẹ́míkà
Ìbọ̀wọ́ rọ́bà2
2
Press, and repeat
Press, and repeat
Press the cream to drive out the liquid. Stir the pressed cake into fresh ether and press again; repeat until no more tannin is removed. Ours: a cloth screw press with filter cloth.
Àwọn irinṣẹ́ tí a nílò:
Ẹ̀rọ ìfún aṣọ oníkọ́kọ́rọ́
Aṣọ ìsẹ́ òwú-àpò tí ó kéré
Diethyl ether
Àpótí eérú (tí ó ní ọ̀pá ìjáde)3
3
Evaporate the pressed liquid (ours)
Evaporate the pressed liquid (ours)
Thorpe gives no work-up. Ours: evaporate the pressed liquid in a dish on a water bath, no flame, to leave the tannic acid.
Àwọn irinṣẹ́ tí a nílò:
Àwo Ìgbẹ
Ìwẹ̀ Omi
Àpótí eérú (tí ó ní ọ̀pá ìjáde)Àwọn ohun-èlò
1- 1 as requiredÀyè
Ìtọ́nisọ́nà yìí ń ṣe
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