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Barium-Strontium Ferrite Disc Magnet: 0.5 mol BaCO3, 0.5 mol SrCO3, 1240 °C (Went, Philips 1956, Ex. 29)
A ceramic magnet with both barium and strontium: 0.5 mol barium carbonate and 0.5 mol strontium carbonate to 2.5 mol iron oxide, milled as in Example 28, pressed and passed through a 1240 °C furnace in 10 minutes. Went's rod held 1,550 gauss with a coercive force of 3,410 oersted.
Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 29. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Abantado
2 days
Mga Tagubilin
1
1
Weigh the carbonates and iron oxide
Weigh the carbonates and iron oxide
Weigh 99.2 g barium carbonate (0.5 mol), 73.8 g strontium carbonate (0.5 mol), 402.0 g ferric oxide (2.5 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.
Mga materyales para sa hakbang na ito:
Barium carbonate (witherite)99.2 g
Strontium carbonate73.8 g
Ferric oxide402 gMga kailangang kasangkapan:
Timbangang panimbang
Gwantes na goma
Panala sa Hininga na P1002
2
Mill with alcohol 15 hours, dry
Mill with alcohol 15 hours, dry
As in Example 28: grind the mixture with alcohol in a ball mill for 15 hours, then dry it.
Mga kailangang kasangkapan:
Gilingang Bolang Bakal
Etanol - antas laboratoryo, 95 %
Hurnong pantuyo3
3
Press the powder
Press the powder
Example 28 moulds a rod without giving the pressure. Ours: press discs at 1.5 tonnes per cm², the pressure of the patent's other examples.
Mga kailangang kasangkapan:
Haydroliko na pandiin
Hulmahan sa pagpindot ng disk4
4
Pass through a 1240 °C zone in 10 minutes
Pass through a 1240 °C zone in 10 minutes
Sinter at 1240 °C by passing the pieces through a 10 cm hot zone at 10 mm per minute: 10 minutes in the heat.
Mga kailangang kasangkapan:
Hurnong Tubo
Guwantes na Matibay sa Init5
5
Magnetise the discs
Magnetise the discs
The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.
Mga kailangang kasangkapan:
Elektromagneto
KompasMga Materyales
3- Placeholder
- 73.8 gPlaceholder
- 402 gPlaceholder
Mga Kinakailangang Kasangkapan
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