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Neodymium Magnets, Sample 22: 73Fe-8B-19Nd Sintered (Sagawa 1988)
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28. Oktubre 2026NO
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Neodymium Magnets, Sample 22: 73Fe-8B-19Nd Sintered (Sagawa 1988)

Neodymium magnets are iron, boron and neodymium. Sagawa's team at Sumitomo melted the three together, ground the casting to a powder finer than 10 µm, lined the grains up in a magnetic field while pressing them, and sintered the compact in argon. This is their sample 22, 73 % iron, 8 % boron and 19 % neodymium by atoms: 28.0 MGOe. Source: M. Sagawa et al. (Sumitomo Special Metals), US 4,770,723 (1988). Unknown: how the pure iron, the ferroboron and the neodymium metal are made; the patent does not say. The magnetising is ours, after Przybylski et al., Sensors 16:569 (2016). The 1 kg weights are our arithmetic from the patent's atomic percentages. Picture: the patent's Fig. 8.
Dalubhasa
2 days

Mga Tagubilin

1

Weigh sample 22: 73 Fe, 8 B, 19 Nd

Sample 22 is 73 % iron, 8 % boron and 19 % neodymium by atoms. Use 99.9 % electrolytic iron, ferroboron (19.38 % B, 5.32 % Al, 0.74 % Si, 0.03 % C, the rest iron) and neodymium of 99.7 % or better. Ours: a 1 kg melt, by arithmetic: 542.3 g iron, 64.6 g ferroboron, 397.0 g neodymium. Unknown: how these three are made.

Mga materyales para sa hakbang na ito:

Elektrolitikong bakalElektrolitikong bakal542.3 g
FerroboronFerroboron64.6 g
Neodymium na metalNeodymium na metal397 g

Mga kailangang kasangkapan:

Timbangang panimbangTimbangang panimbang
2

Melt by high frequency in argon and cast

Melt the charge in a high-frequency (induction) furnace under argon and pour it into a water-cooled copper mould.

Mga kailangang kasangkapan:

Induction furnaceInduction furnace
Krisol na Luwad na Matibay sa ApoyKrisol na Luwad na Matibay sa Apoy
ArgonArgon
Tangke ng gas na may presyonTangke ng gas na may presyon
Hulmahang tanso na pinalalamig ng tubigHulmahang tanso na pinalalamig ng tubig
Guwantes na Matibay sa InitGuwantes na Matibay sa Init
3

Stamp to 35 mesh, ball-mill to 3-10 µm

Crush the casting in a stamp mill until it passes a 35-mesh sieve. Then grind it in a ball mill for 3 hours, to 3-10 µm.

Mga kailangang kasangkapan:

Galingang PandurogGalingang Pandurog
Set ng salaan (sunod-sunod na butas)Set ng salaan (sunod-sunod na butas)
Gilingang Bolang BakalGilingang Bolang Bakal
Salaming pangkaligtasanSalaming pangkaligtasan
4

Press in a 10 kOe field at 1.5 t/cm²

Line the powder up in a magnetic field of 10 kOe and press it at 1.5 tonnes per cm². Unknown: the size and shape of the magnets.

Mga kailangang kasangkapan:

Pindutang may magnetic fieldPindutang may magnetic field
5

Sinter in argon at 1000-1200 °C

Sinter the compacts at 1000-1200 °C for about one hour in argon, then let them cool. Sample 22 measured 10.9 kG remanence, 11.4 kOe coercivity and 28.0 MGOe.

Mga kailangang kasangkapan:

Hurnong TuboHurnong Tubo
ArgonArgon
Tangke ng gas na may presyonTangke ng gas na may presyon
Guwantes na Matibay sa InitGuwantes na Matibay sa Init
6

Magnetise the magnets

Ours, after Przybylski et al., Sensors 16:569 (2016): put each magnet in the coil of an impulse magnetiser and discharge a capacitor bank through it. They found a field of 1200 kA/m enough to saturate N38 sintered Nd-Fe-B; their magnetiser used a 1 mF bank charged up to 5000 V, a thyristor switch and a 440-turn coil of 3 mm copper wire with an 80 mm bore.

Mga kailangang kasangkapan:

MagnetizerMagnetizer

Mga Materyales

3

Mga Kinakailangang Kasangkapan

14

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