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Strontium Ferrite Disc Magnet: Presintered at 1100 °C, 0.1 mol SrCO3 to 0.7 mol Iron Oxide (Went, Philips 1956, Ex. 8)
A strontium ferrite: 0.1 mol strontium carbonate to 0.7 mol iron oxide, dried, milled, presintered 3.5 hours at 1100 °C, bound, formed and passed through a 1280 °C furnace in 10 minutes. Went's rod held 1,535 gauss with a coercive force of 2,800 oersted.
Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 8. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Abantado
2 days
Mga Tagubilin
1
1
Weigh strontium carbonate and iron oxide
Weigh strontium carbonate and iron oxide
Weigh 14.8 g strontium carbonate (0.1 mol) and 112.1 g ferric oxide (0.7 mol).
Mga materyales para sa hakbang na ito:
Strontium carbonate14.8 g
Ferric oxide112.1 gMga kailangang kasangkapan:
Timbangang panimbang
Panala sa Hininga na P1002
2
Dry at 200 °C, mill with alcohol 4 hours
Dry at 200 °C, mill with alcohol 4 hours
Dry the mixture at 200 °C, then grind it with alcohol in a ball mill for 4 hours and dry it.
Mga kailangang kasangkapan:
Hurnong pantuyo
Gilingang Bolang Bakal
Etanol - antas laboratoryo, 95 %3
3
Presinter in air at 1100 °C for 3.5 hours
Presinter in air at 1100 °C for 3.5 hours
Fire the powder in air at 1100 °C for about 3.5 hours.
Mga kailangang kasangkapan:
Muffle furnace
Krisol na may takip (porselana)
Sipit ng Krisol
Guwantes na Matibay sa Init4
4
Add a binder and form, dry overnight
Add a binder and form, dry overnight
Add a binder as in Example 1 (polyvinyl alcohol or nitrocellulose). The patent extrudes rods; ours: press discs at 1.5 tonnes per cm². Dry overnight.
Mga kailangang kasangkapan:
Pulbos na polyvinyl alcohol
Haydroliko na pandiin
Hulmahan sa pagpindot ng diskHurnong pantuyo5
5
Pass through a 1280 °C zone in 10 minutes
Pass through a 1280 °C zone in 10 minutes
Sinter in air at 1280 °C by passing the pieces through a 10 cm hot zone at 10 mm per minute: 10 minutes in the heat.
Mga kailangang kasangkapan:
Hurnong TuboGuwantes na Matibay sa Init6
6
Magnetise the discs
Magnetise the discs
The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.
Mga kailangang kasangkapan:
Elektromagneto
KompasMga Materyales
2- 14.8 gPlaceholder
- 112.1 gPlaceholder
Mga Kinakailangang Kasangkapan
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