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Metal Oxide Varistor: Zinc Oxide with Bismuth, Manganese and Barium Oxides, 1350 °C (Masuyama 1972, Ex. 3)
Masuyama, Matsuoka and Nishi found that adding two more oxides to zinc oxide and bismuth oxide gives excellent non-linear properties. This is their Example 3 with manganese dioxide and barium oxide: 98.5 % zinc oxide and 0.5 % each of bismuth oxide, manganese dioxide and barium oxide by moles, sintered at 1350 °C. The disc measured a C-value of 73 at 1 mA and a nonlinearity exponent n of 21.5.
Source: T. Masuyama, M. Matsuoka and T. Nishi (Matsushita), US 3,663,458 (1972), Example 3. Unknown: what the silver paint is. The spraying is ours, after US Army Corps of Engineers EM 1110-2-3401 (1999). The 10 g batch is our arithmetic. Picture: the patent's drawing.
Abantado
1 day
Mga Tagubilin
1
1
Weigh 98.5 : 0.5 : 0.5 : 0.5 and wet-mill 5 hours
Weigh 98.5 : 0.5 : 0.5 : 0.5 and wet-mill 5 hours
Mix zinc oxide, bismuth oxide, manganese dioxide and barium oxide 98.5 : 0.5 : 0.5 : 0.5 by moles. Ours, for 10 g: 9.578 g zinc oxide, 0.278 g bismuth oxide, 0.052 g manganese dioxide, 0.092 g barium oxide (our arithmetic). Mill wet for 5 hours, then dry. Unknown: the milling liquid.
Mga materyales para sa hakbang na ito:
Pulbos ng Zinc Oxide9.578 g
Bismuth oxide0.278 g
Manganese dioxide (pirolusita)0.052 g
Barium oxide0.092 gMga kailangang kasangkapan:
Timbangang panimbang
Gilingang Bolang Bakal
Hurnong pantuyo2
2
Press discs 13 mm by 2.5 mm
Press discs 13 mm by 2.5 mm
Press the powder in a mould into discs 13 mm across and 2.5 mm thick at 340 kg/cm², as in Example 1.
Mga kailangang kasangkapan:
Haydroliko na pandiin
Hulmahan sa pagpindot ng disk
Kalipers na Vernier3
3
Sinter 1 hour at 1350 °C and furnace-cool
Sinter 1 hour at 1350 °C and furnace-cool
Sinter the discs in air at 1350 °C for 1 hour, then let them cool in the furnace to room temperature (about 15-30 °C).
Mga kailangang kasangkapan:
Muffle furnace4
4
Lap to 10 mm by 1.5 mm
Lap to 10 mm by 1.5 mm
Lap both faces with 600-mesh silicon carbide. The finished disc is 10 mm across and 1.5 mm thick.
Mga kailangang kasangkapan:
Butil ng silicon carbideKalipers na Vernier5
5
Spray aluminium electrodes and attach leads
Spray aluminium electrodes and attach leads
Spray a metallised film of aluminium on both faces. Attach a lead wire to each with conductive silver paint. Ours, after US Army Corps of Engineers EM 1110-2-3401 (1999): wire-arc spray the aluminium from two 3.2 mm wires melted by an 18-40 V DC arc and atomised by compressed air, 15-20 cm from the disc and never at less than 45°, in at least two coats at right angles of 50-75 µm each. Unknown: the paint.
Mga materyales para sa hakbang na ito:
Bareta ng aluminyo1 as 3.2 mm spray wire
Pinturang pilak na nagdadala ng kuryente1 as required
Kawad na Tanso2 pirasoMga kailangang kasangkapan:
Kalipers na Vernier
Baril na pang-spray na may arko ng kawad
Pang-industriyang panipil ng hanginMga Materyales
7- 9.578 gPlaceholder
- 0.278 gPlaceholder
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- 0.092 gPlaceholder
- 1 as 3.2 mm spray wirePlaceholder
- 1 as requiredPlaceholder
- 2 pirasoPlaceholder
Mga Kinakailangang Kasangkapan
10- Placeholder
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