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Ionisation Gauge
Ed

Autor

Ed

26. sierpień 2026FI
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Ionisation Gauge

Below the Pirani gauge's floor there is almost nothing left to measure — so few molecules that they no longer conduct heat, deflect a diaphragm or do anything mechanical at all. The ionisation gauge counts them instead. A hot filament emits electrons, those electrons are accelerated and collide with whatever gas remains, knocking electrons off molecules to make positive ions; a collector electrode gathers those ions and the current it receives is proportional to how many molecules were there to ionise. Bayard and Alpert's 1950 refinement, replacing the fat central collector with a fine wire, extended the range by orders of magnitude and made ultra-high vacuum measurable at all.
Zaawansowany
5 hours

Instrukcje

1

Build the three-electrode structure

Filament, grid and collector — the same architecture as a triode valve, doing a different job.

  1. Mount a fine tungsten filament as the electron source.
  2. Surround it with an open helical grid of wire, which will be held at a positive voltage.
  3. Place a collector electrode outside the grid.
  4. Bring three separate feedthroughs out of the envelope.
  5. Check none of the electrodes can touch another.

This is a Fleming valve with an extra electrode and an opposite purpose. A valve is built to have as little gas inside as possible so the electron stream is undisturbed; an ionisation gauge is built to measure the small amount that remains by deliberately letting electrons collide with it. The same structure, optimised for opposite ends.

Fine wire everywhere. A thick collector intercepts soft X-rays produced when electrons strike the grid, and those X-rays release electrons from the collector that look exactly like ion current — which sets a false floor to the reading.

Materiały do tego kroku:

Enamelled Copper WireEnamelled Copper Wire1 rolka
Glass Tubing KitGlass Tubing Kit1 zestaw
Bare Copper Wire 10 AWGBare Copper Wire 10 AWG1 rolka

Tools needed:

Digital Multimeter (Lab Grade)Digital Multimeter (Lab Grade)
File SetFile Set
Digital Caliper 6-InchDigital Caliper 6-Inch
Bench Vise (4-inch, Cast Iron)Bench Vise (4-inch, Cast Iron)
2

Set the three voltages correctly

Each electrode has a job, and the voltages are what assign them.

  1. Heat the filament until it emits — a low voltage at significant current.
  2. Hold the grid strongly POSITIVE, so electrons are accelerated toward and through it.
  3. Hold the collector slightly NEGATIVE, so it repels electrons but attracts positive ions.
  4. Measure the collector current with a sensitive meter.

The collector must reject electrons and accept ions. Making it slightly negative does both: electrons are turned back, positive ions are drawn in. Without that discrimination the collector would receive a huge electron current that swamps the tiny ion current entirely — the signal is often a millionth of the electron current or less.

Regulate the filament emission. The ion current is proportional to both the pressure AND the number of electrons available to do the ionising, so an unstable filament makes the reading drift for reasons that have nothing to do with vacuum.

Materiały do tego kroku:

Adjustable Bench Power Supply (30V/5A)Adjustable Bench Power Supply (30V/5A)1 sztuka
1/4W Resistor Kit (600pcs, 30 Values)1/4W Resistor Kit (600pcs, 30 Values)1 zestaw

Tools needed:

Digital Multimeter (Lab Grade)Digital Multimeter (Lab Grade)
Analog MultimeterAnalog Multimeter
Digital Caliper 6-InchDigital Caliper 6-Inch
3

Read pressure where the Pirani is blind

Run both gauges together across the whole pump-down and watch the handover.

  1. Fit the Pirani and the ionisation gauge on the same system.
  2. Start the backing pump and record both from atmosphere.
  3. Note where the Pirani flattens and stops responding.
  4. Start the diffusion pump and continue recording the ionisation gauge alone.
  5. Plot both on one logarithmic pressure axis.
The two curves overlap in a narrow band and then the Pirani goes flat while the ionisation gauge carries on for several more decades of pressure. Real vacuum systems fit both for exactly this reason, and the overlap region is where you check that they agree. No single gauge covers the full range from atmosphere to ultra-high vacuum — a span of thirteen orders of magnitude — and pretending otherwise is how people misread their systems.

Materiały do tego kroku:

Graph PaperGraph Paper1 pad

Tools needed:

Digital Multimeter (Lab Grade)Digital Multimeter (Lab Grade)
StopwatchStopwatch
Digital Caliper 6-InchDigital Caliper 6-Inch
4

Discover that the gauge is also a pump

An instrument that changes what it measures — the classic instrumentation trap.

  1. Isolate a small volume with the gauge running and the pumps valved off.
  2. Record the indicated pressure over twenty minutes.
  3. Note that it FALLS, with no pump connected.
  4. Switch the gauge off for ten minutes, switch it back on and read again.
The gauge is pumping: ions driven into the collector and walls are buried there, and the hot filament getters reactive gases exactly like the barium film in the previous blueprint. So a running ionisation gauge slowly removes the gas it is trying to measure, and in a small sealed volume it reports a pressure lower than the true one. Every measurement disturbs its subject; here the disturbance is large enough to matter, and knowing that is the difference between a reading and an interpretation.

Tools needed:

Digital Multimeter (Lab Grade)Digital Multimeter (Lab Grade)
StopwatchStopwatch
5

Counting what is barely there, and history

The hot-cathode ionisation gauge dates from around 1916, but its useful floor was limited by a phenomenon nobody understood until Robert Bayard and Daniel Alpert identified it in 1950. Electrons striking the grid produce soft X-rays; those X-rays strike the collector and eject photoelectrons; that current is indistinguishable from ion current and does not depend on pressure at all. It set a false floor.

Their fix was geometric and beautifully simple: make the collector a very fine wire rather than a large cylinder, so it presents almost no area for X-rays to strike, and move the filament outside the grid. The X-ray limit dropped by orders of magnitude, and pressures previously unmeasurable became routine. The Bayard-Alpert gauge is still the standard ultra-high-vacuum instrument seventy-five years later.

Where it sits in the chain: the McLeod gauge is a primary standard but slow, manual and blind to vapours. The Pirani reads continuously but saturates. The ionisation gauge reads far lower than either, continuously and electrically — but it is not a primary standard, it depends on the gas species, and it perturbs the system. Three gauges, three regions, and a real system carries at least two.

Its honest limits: gas-dependent sensitivity; the pumping effect from step 4; a filament that can burn out if exposed to air while hot; and contamination of the electrodes changing the calibration. It also cannot be used above a certain pressure at all, because the filament oxidises — which is why it must be interlocked to switch off if the vacuum is lost.

Materiały

6

Wymagane narzędzia

6

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