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Barium-Calcium Ferrite Disc Magnet: 0.09 mol BaCO3 and 0.01 mol CaCO3 (Went, Philips 1956, Ex. 19)
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28. Ukwakira 2026DE
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Barium-Calcium Ferrite Disc Magnet: 0.09 mol BaCO3 and 0.01 mol CaCO3 (Went, Philips 1956, Ex. 19)

A ceramic magnet with a tenth of the barium replaced by calcium: 0.09 mol barium carbonate and 0.01 mol calcium carbonate to 0.6 mol iron oxide, made as in Example 18: milled, presintered at 1000 °C, milled again, formed and passed through a 1330 °C furnace in 10 minutes. Went's rod held 1,705 gauss with a coercive force of 1,110 oersted. Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 19. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Hejuru
2 days

Amabwiriza

1

Weigh barium carbonate, chalk and iron oxide

Weigh 17.76 g barium carbonate (0.09 mol), 1.001 g calcium carbonate (0.01 mol) and 95.55 g ferric oxide (0.6 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.

Ibikoresho by'iyi ntambwe:

Karubonate ya bariyumu (witerite)Karubonate ya bariyumu (witerite)17.76 g
Kaboneti ya kalisiyumu (ifu y'umweru)Kaboneti ya kalisiyumu (ifu y'umweru)1.001 g
Oxide ya feriOxide ya feri95.55 g

Ibikoresho bikenewe:

Umunzani w'ibiroUmunzani w'ibiro
Uturindantoki tw'ikawusuUturindantoki tw'ikawusu
Agapfukamunwa ka P100Agapfukamunwa ka P100
2

Mill with alcohol 4 hours, dry at 150 °C

Grind with alcohol in a ball mill for 4 hours and dry in air at 150 °C.

Ibikoresho bikenewe:

Urusyo rw'imipira y'icyumaUrusyo rw'imipira y'icyuma
Etanoli - urwego rw'ubushakashatsi, 95 %Etanoli - urwego rw'ubushakashatsi, 95 %
Ifuru yo kumishahoIfuru yo kumishaho
3

Presinter in air at 1000 °C for 2 hours

Fire in air at 1000 °C for 2 hours.

Ibikoresho bikenewe:

Ifuru ya muffleIfuru ya muffle
Ikirundo cyo gushongeramo gifite igifuniko (porukorene)Ikirundo cyo gushongeramo gifite igifuniko (porukorene)
Amakoro y'Icyombo GishongeshaAmakoro y'Icyombo Gishongesha
Uturindantoki twihanganira ubushyuheUturindantoki twihanganira ubushyuhe
4

Mill again 4 hours, dry, form

Grind again with alcohol for 4 hours and dry. Example 19 extrudes a rod; ours: press discs at 1.5 tonnes per cm², as Example 18 moulds its rod.

Ibikoresho bikenewe:

Urusyo rw'imipira y'icyumaUrusyo rw'imipira y'icyuma
Etanoli - urwego rw'ubushakashatsi, 95 %Etanoli - urwego rw'ubushakashatsi, 95 %
Ifuru yo kumishahoIfuru yo kumishaho
Imashini ikanda ikoresha amaziImashini ikanda ikoresha amazi
Ifumbiro ryo gukanda disikiIfumbiro ryo gukanda disiki
5

Pass through a 1330 °C zone in 10 minutes

Sinter at 1330 °C by passing the pieces through a 10 cm hot zone at 10 mm per minute: 10 minutes in the heat.

Ibikoresho bikenewe:

Itanura ry'umuyoboroItanura ry'umuyoboro
Uturindantoki twihanganira ubushyuheUturindantoki twihanganira ubushyuhe
6

Magnetise the discs

The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.

Ibikoresho bikenewe:

Iroha ry'amashanyaraziIroha ry'amashanyarazi
IkirangamurongoIkirangamurongo

Ibikoresho

3

Ibikoresho bikenewe

15

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