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Barium-Calcium Ferrite Disc Magnet: 20 % Calcium, 5 Minutes at 1290 °C (Went, Philips 1956, Ex. 20)
A ceramic magnet with a fifth of the barium replaced by calcium: 0.08 mol barium carbonate, 0.02 mol calcium carbonate and 0.6 mol iron oxide, made as in Example 18 but sintered at 1290 °C for only 5 minutes. Went's rod held 1,615 gauss with a coercive force of 1,550 oersted.
Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 20. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Hejuru
2 days
Amabwiriza
1
1
Weigh barium carbonate, chalk and iron oxide
Weigh barium carbonate, chalk and iron oxide
Weigh 15.79 g barium carbonate (0.08 mol), 2.002 g calcium carbonate (0.02 mol) and 95.55 g ferric oxide (0.6 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.
Ibikoresho by'iyi ntambwe:
Karubonate ya bariyumu (witerite)15.79 g
Kaboneti ya kalisiyumu (ifu y'umweru)2.002 g
Oxide ya feri95.55 gIbikoresho bikenewe:
Umunzani w'ibiro
Uturindantoki tw'ikawusu
Agapfukamunwa ka P1002
2
Mill, presinter and mill as in Example 18
Mill, presinter and mill as in Example 18
As in Example 18: grind with alcohol 4 hours, dry at 150 °C, fire in air at 1000 °C for 2 hours, grind again 4 hours and dry.
Ibikoresho bikenewe:
Urusyo rw'imipira y'icyuma
Etanoli - urwego rw'ubushakashatsi, 95 %
Ifuru yo kumishaho
Ifuru ya muffle
Ikirundo cyo gushongeramo gifite igifuniko (porukorene)
Amakoro y'Icyombo Gishongesha3
3
Press at 1.5 t/cm²
Press at 1.5 t/cm²
Press at 1.5 tonnes per cm², as in Example 18 (ours: discs instead of rods).
Ibikoresho bikenewe:
Imashini ikanda ikoresha amazi
Ifumbiro ryo gukanda disiki4
4
Pass through a 1290 °C zone in 5 minutes
Pass through a 1290 °C zone in 5 minutes
Sinter in air at 1290 °C by passing the pieces through a 10 cm hot zone at 20 mm per minute: 5 minutes in the heat.
Ibikoresho bikenewe:
Itanura ry'umuyoboro
Uturindantoki twihanganira ubushyuhe5
5
Magnetise the discs
Magnetise the discs
The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.
Ibikoresho bikenewe:
Iroha ry'amashanyarazi
IkirangamurongoIbikoresho
3- Umwanya
- Umwanya
- 95.55 gUmwanya
Ibikoresho bikenewe
15- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
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