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Barium Ferrite Disc Magnet: Fired in Carbon Dioxide, Pressed at 12 t/cm² (Went, Philips 1956, Ex. 33)
A barium ferrite made with more iron oxide, 0.4 mol barium carbonate to 3.6 mol, fired an hour at 1300 °C in carbon dioxide. Little oxygen gives the hexagonal crystal BaFe18O27, with some iron in the lower state. It is milled again, bound with nitrocellulose or polyvinyl alcohol, and pressed hard at 12 tonnes per cm². Went's rod held 1,260 gauss with a coercive force of 700 oersted.
Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 33. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Hejuru
2 days
Amabwiriza
1
1
Weigh barium carbonate and iron oxide
Weigh barium carbonate and iron oxide
Weigh 79.4 g barium carbonate (0.4 mol) and 580.9 g ferric oxide (3.6 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.
Ibikoresho by'iyi ntambwe:
Karubonate ya bariyumu (witerite)79.4 g
Oxide ya feri580.9 gIbikoresho bikenewe:
Umunzani w'ibiro
Uturindantoki tw'ikawusu
Agapfukamunwa ka P1002
2
Mill 15.5 hours, press a pastille, fire in CO2
Mill 15.5 hours, press a pastille, fire in CO2
Grind with alcohol in a ball mill for 15.5 hours, dry, and press into a pastille. Heat it at 1300 °C in carbon dioxide for 1 hour (ours: a tube furnace fed from a CO2 cylinder).
Ibikoresho bikenewe:
Urusyo rw'imipira y'icyuma
Etanoli - urwego rw'ubushakashatsi, 95 %
Ifuru yo kumishaho
Imashini ikanda ikoresha amazi
Ifumbiro ryo gukanda disiki
Itanura ry'umuyoboro
Gaze ya dioxyde de carbone
Ibariro rya gazi ifite igitutu
Uturindantoki twihanganira ubushyuhe3
3
Pulverise, mill 14 hours, bind
Pulverise, mill 14 hours, bind
Crush the cooled pastille and grind it with alcohol for 14 hours. Press the powder into a pastille again with a ceramic binder (ours: polyvinyl alcohol, one of the two named), then crush it to grains.
Ibikoresho by'iyi ntambwe:
Ifu ya polyvinyl alcohol1 as requiredIbikoresho bikenewe:
Urusyo rw'imipira y'icyuma
Etanoli - urwego rw'ubushakashatsi, 95 %
Imashini ikanda ikoresha amazi
Ifumbiro ryo gukanda disiki4
4
Press at 12 tonnes per cm²
Press at 12 tonnes per cm²
Press the grains at 12 tonnes per cm² (ours: discs instead of rods). The patent describes no further firing.
Ibikoresho bikenewe:
Imashini ikanda ikoresha amazi
Ifumbiro ryo gukanda disiki5
5
Magnetise the discs
Magnetise the discs
The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.
Ibikoresho bikenewe:
Iroha ry'amashanyarazi
IkirangamurongoIbikoresho
3- Umwanya
- 580.9 gUmwanya
- 1 as requiredUmwanya
Ibikoresho bikenewe
14- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
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