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Barium Ferrite Disc Magnet from Natural Magnetite, Presintered at 900 °C (Went, Philips 1956, Ex. 36, Procedure 1)
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28. Ukwakira 2026DE
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Barium Ferrite Disc Magnet from Natural Magnetite, Presintered at 900 °C (Went, Philips 1956, Ex. 36, Procedure 1)

A barium ferrite magnet made from natural magnetite instead of ferric oxide: barium carbonate and magnetite ground 18 hours, presintered 3 hours at 900 °C, ground again 18 hours, pressed and sintered 2 hours at 1200 °C. Went's rod held 1,450 gauss with a coercive force of 2,425 oersted. Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 36. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Hejuru
2 days

Amabwiriza

1

Weigh barium carbonate and magnetite

Weigh 9.9 g barium carbonate (0.05 mol) and 46.9 g natural magnetite, Fe3O4 (0.20 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.

Ibikoresho by'iyi ntambwe:

Karubonate ya bariyumu (witerite)Karubonate ya bariyumu (witerite)9.9 g
ManyetiteManyetite46.9 g

Ibikoresho bikenewe:

Umunzani w'ibiroUmunzani w'ibiro
Uturindantoki tw'ikawusuUturindantoki tw'ikawusu
Agapfukamunwa ka P100Agapfukamunwa ka P100
2

Grind 18 hours in a ball mill

Grind the mixture in a ball mill for 18 hours. The patent does not say whether wet or dry.

Ibikoresho bikenewe:

Urusyo rw'imipira y'icyumaUrusyo rw'imipira y'icyuma
Agapfukamunwa ka P100Agapfukamunwa ka P100
3

Presinter at 900 °C for 3 hours

Fire the ground mixture at 900 °C for three hours and let it cool.

Ibikoresho bikenewe:

Ifuru ya muffleIfuru ya muffle
Ikirundo cyo gushongeramo gifite igifuniko (porukorene)Ikirundo cyo gushongeramo gifite igifuniko (porukorene)
Amakoro y'Icyombo GishongeshaAmakoro y'Icyombo Gishongesha
Uturindantoki twihanganira ubushyuheUturindantoki twihanganira ubushyuhe
4

Grind 18 hours in a ball mill

Grind it again in a ball mill for 18 hours. The patent does not say whether wet or dry.

Ibikoresho bikenewe:

Urusyo rw'imipira y'icyumaUrusyo rw'imipira y'icyuma
Agapfukamunwa ka P100Agapfukamunwa ka P100
5

Press at 1.5 t/cm²

Press at 1.5 tonnes per cm² (ours: discs instead of a rod).

Ibikoresho bikenewe:

Imashini ikanda ikoresha amaziImashini ikanda ikoresha amazi
Ifumbiro ryo gukanda disikiIfumbiro ryo gukanda disiki
6

Sinter at 1200 °C for 2 hours

Sinter at 1200 °C for 2 hours. The patent gives no atmosphere for this example. Went's rod: 1,450 gauss, 2,425 oersted.

Ibikoresho bikenewe:

Ifuru ya muffleIfuru ya muffle
Amakoro y'Icyombo GishongeshaAmakoro y'Icyombo Gishongesha
Uturindantoki twihanganira ubushyuheUturindantoki twihanganira ubushyuhe
7

Magnetise the discs

The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.

Ibikoresho bikenewe:

Iroha ry'amashanyaraziIroha ry'amashanyarazi
IkirangamurongoIkirangamurongo

Ibikoresho

2

Ibikoresho bikenewe

12

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