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Ceramic Disc Capacitors: Barium Titanate with Nickel Stannate, Pressed, Fired and Silvered (Coffeen, US 2,789,061)
Barium titanate with 3 mole % nickel stannate is calcined, pressed into small discs and fired hard. Silver is fired onto both faces and a lead soldered to each, giving ceramic disc capacitors of high capacity for their size.
Result: discs 3/8 inch across and about 1/10 inch thick with a dielectric constant averaging 2380 and a dissipation factor of 0.58 %. Between 25 and 85 °C the dielectric constant rose at most 17 % and fell at most 7 %.
Source: W. W. Coffeen (Metal & Thermit Corp.), US 2,789,061 (1957). Unknown: how the barium titanate, the nickel stannate and the tinned lead wire are made; the patent uses them ready-made. Picture: Wikimedia Commons.
Hejuru
10 days
Amabwiriza
1
1
Weigh and slurry
Weigh and slurry
Weigh 19.32 g of barium titanate and 0.68 g of hydrated nickel stannate (about NiSnO3·2H2O), which is 97 mole % BaTiO3 and 3 mole % NiSnO3. Slurry them with 50 cc of distilled water. The patent prefers 2 to 4 mole % nickel stannate; 1 to 15 % works.
Ibikoresho by'iyi ntambwe:
Bariyumu titanate19.32 g
Nikeli sitanate0.68 gIbikoresho bikenewe:
Amazi Yatunganyijwe
Iminzani ya Digitale Nyayo
Isahani yo kumisha2
2
Dry, sieve and calcine
Dry, sieve and calcine
Dry the slurry, crush it to pass a 50 mesh screen, moisten it with 5 % of a 2 1/2 % starch solution and press it into one slug. Calcine the slug for one hour at 1600 °F (871 °C). Ours: potato starch, a drying oven, mortar and pestle.
Ibikoresho bikenewe:
Amidoni y'ibirayi
Ifuru yo kumishaho
Isekuru n'Umuhini
Akayungurizo
Imashini ikanda ikoresha amazi
Itanura ry'ubushyuhe bwinshi3
3
Press the discs
Press the discs
Grind the calcine to pass a 325 mesh screen, moisten it again with starch solution, and press small discs 3/8 inch in diameter and about 1/10 inch thick at 20,000 pounds per square inch.
Ibikoresho bikenewe:
Isekuru n'Umuhini
Akayunguruzo Gafite Urukoma Ruto
Amidoni y'ibirayi
Imashini ikanda ikoresha amazi
Ifumbiro ryo gukanda disiki4
4
Fire on platinum
Fire on platinum
Fire the discs on platinum foil at 2400 °F (1316 °C) for one hour. They come out with zero absorption.
Ibikoresho bikenewe:
Itanura ry'ubushyuhe bwinshi
Platine5
5
Silver and lead
Silver and lead
Paint silver paint on both faces and fire the discs at 1350 °F (732 °C) for one hour. Solder tinned copper lead wires directly to the silver electrodes. Age at least a week before measuring. Ours: a fine brush and a soldering iron.
Ibikoresho by'iyi ntambwe:
Irangi rya feza ryotswa1 both faces
Insinga y’umuringa isizweho sitani2 leads per disc
Urusinga rw'isudire1 a littleIbikoresho bikenewe:
Imikino ifite impera zoroheje
Itanura ry'ubushyuhe bwinshi
Icyuma cyo gusudiraIbikoresho
5- 19.32 gUmwanya
- 0.68 gUmwanya
- 1 both facesUmwanya
- 2 leads per discUmwanya
- 1 a littleUmwanya
Ibikoresho bikenewe
14- Umwanya
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- 2 vendors sell this, none ship to you yetUmwanya
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