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Lactic Acid: Wackenroder's Calcium Lactate Split with Oxalic Acid (US Dispensatory 1907)
Wackenroder's lactic acid: skimmed milk, milk sugar, chalk and water kept warm for a month. As the acid forms, the chalk takes it up as calcium lactate. That salt is crystallised and then split with exactly enough oxalic acid to free the lactic acid; the lime falls as calcium oxalate.
Source: The Dispensatory of the United States of America (1907), Acidum Lacticum. Pharmacopoeial lactic acid, used as food-grade, as ruled. Unknown: how the free acid is separated afterwards; the Dispensatory does not say, so it is linked to an unknown head. The sulphuric-acid version is a separate blueprint. Picture drawn by Youblob.
Hagati
5 weeks
Amabwiriza
1
1
Mix 10 : 2.5 : 2 : 20
Mix 10 : 2.5 : 2 : 20
Mix 10 parts skimmed milk, 2.5 parts milk sugar, 2 parts chalk and 20 parts water. Ours: grams.
Ibikoresho by'iyi ntambwe:
Amata avanyweho amavuta10 parts
Isukari y’amata2.5 parts
Kaboneti ya kalisiyumu (ifu y'umweru)2 parts
Amazi20 partsIbikoresho bikenewe:
Umunzani w'ibiro
Ikibindi cy'ikirahure2
2
Digest at about 24 °C for a month
Digest at about 24 °C for a month
Keep it at about 23.8 °C (75 °F) for a month, or until the chalk has dissolved.
Ibikoresho bikenewe:
Ikibindi cy'ikirahure
Igipima Ubushyuhe cy'Ubushakashatsi3
3
Press, clarify and crystallise the calcium lactate
Press, clarify and crystallise the calcium lactate
Press it out, clarify it, and evaporate it so the calcium lactate crystallises. Recrystallise it.
Ibikoresho bikenewe:
Umwenda wa fromaji
Urupapuro rwo Kuyungurura
Isahani yo kumisha
Urubaho rushyushya4
4
Split the salt with oxalic acid
Split the salt with oxalic acid
Decompose the calcium lactate with oxalic acid in exactly the saturating proportion. Oxalic acid is poisonous if swallowed: gloves. Unknown: how the lactic acid is then separated.
Ibikoresho by'iyi ntambwe:
Asiide ya oxalike dihidirate1 as requiredIbikoresho bikenewe:
Ikibindi cy'ikirahure
Itunganya ritazwi
Amadarubindi yo Kwirinda Ibinyabutabire
Uturindantoki twa NitirileIbikoresho
5- 10 partsUmwanya
- 2.5 partsUmwanya
- Umwanya
- 20 partsUmwanya
- 1 as requiredUmwanya
Ibikoresho bikenewe
10- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
Iki gishushanyo gikora
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