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Youblob (drawn after Fownes) · CC0
Potassium Sulfate from the Nitric Acid Residue
When nitric acid is distilled from saltpetre and sulfuric acid, an acid salt is left in the retort. George Fownes's chemistry manual turns it into potassium sulfate: dissolve it, neutralise it with crude potash and let the neutral salt crystallise. Potassium sulfate is what makes potash alum from alum shale.
Hagati
A day with cooling
Amabwiriza
1
1
Dissolve the residue
Dissolve the residue
Break the cold residue out of the nitric acid retort and dissolve it in hot water.
Ibikoresho by'iyi ntambwe:
Bisulfate ya potasiyumu500 g
Amazi2 litiroIbikoresho bikenewe:
Umunzani w'ibiro
Igikombe cy'Ikirahure
Urubaho rushyushya
Amadarubindi yo Kwirinda Ibinyabutabire
Uturindantoki tw'ikawusu2
2
Neutralise with potash
Neutralise with potash
Stir in crude potash a little at a time; it fizzes. Stop when litmus paper no longer turns red.
Ibikoresho by'iyi ntambwe:
Karubonate ya potasiyumu (potashi)260 gIbikoresho bikenewe:
Igikombe cy'Ikirahure
Urupapuro rwa litimusi
Amadarubindi yo Kwirinda Ibinyabutabire
Uturindantoki tw'ikawusu3
3
Filter and crystallise
Filter and crystallise
Filter it hot, boil it down a little and let it cool. Hard, clear crystals of potassium sulfate form.
Ibikoresho bikenewe:
Akayunguruzo k'Ikirahure Gafite Umugozi
Urupapuro rwo Kuyungurura
Isahani yo kumisha
Urubaho rushyushya4
4
Recrystallise
Recrystallise
Dissolve the crystals again in as little boiling water as will take them, and cool. Dry them gently: Fownes notes they crackle apart if heated suddenly.
Ibikoresho by'iyi ntambwe:
Amazi1 as requiredIbikoresho bikenewe:
Isahani yo kumisha
Urubaho rushyushya5
5
Potash to neutralise the residue
Potash to neutralise the residue
Gupakira ikaye ya Jupyter…
6
6
Limits
Limits
Fownes's method; the amounts are ours, from the reaction. Crude potash carries other salts, so a second crystallising matters.
Ibikoresho
3- Umwanya
- 1 as requiredUmwanya
- Umwanya
Ibikoresho bikenewe
9- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
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