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PTFE Disc: Sintered in a Molten Nitrate Bath, Cooled Slowly (Brubaker & Hanford 1946)
English
Emma

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Emma

27. Ukwakira 2026SE
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PTFE Disc: Sintered in a Molten Nitrate Bath, Cooled Slowly (Brubaker & Hanford 1946)

A PTFE disc pressed cold, then sintered by dipping it in molten salt at 380 °C for half an hour. Instead of being quenched, it cools slowly between magnesite blocks. The patent says slowly cooled pieces are a little softer and less stiff, which is often better for machining. Source: M. M. Brubaker and W. E. Hanford (du Pont), US 2,400,099 (1946), Example II. The patent gives no nitrate-to-nitrite ratio. The mould, press, pot and burner are ours. Picture drawn by Youblob.
Hejuru
1 day

Amabwiriza

1

Press a disc at 500 psi

At 25 °C, press PTFE powder at 500 lb/sq in into a disc 2 in across and ⅜ in thick.

Ibikoresho by'iyi ntambwe:

Ifu ya rezine ya PTFEIfu ya rezine ya PTFE1 as required for the disc

Ibikoresho bikenewe:

Ikibumbiro cyo gukandaIkibumbiro cyo gukanda
Imashini ikanda ikoresha amaziImashini ikanda ikoresha amazi
Umurongo w'ipimaUmurongo w'ipima
2

Melt the salt bath at 380 °C

Melt a mixture of sodium nitrate and sodium nitrite and hold it at 380 °C. The patent gives no ratio. Ours: a cast iron pot on a gas burner.

Ibikoresho bikenewe:

Nitiri ya Shili (nitarate ya sodiyumu)Nitiri ya Shili (nitarate ya sodiyumu)
Nitirite ya sodiyumuNitirite ya sodiyumu
Inkono y'icyuma cyasuweInkono y'icyuma cyasuwe
Igicanwa cya gaziIgicanwa cya gazi
Termokupuli ifite igaragazaTermokupuli ifite igaragaza
3

Dip the disc for half an hour

Lower the pressed disc into the molten bath and leave it there for ½ hour.

Ibikoresho bikenewe:

Igikoresho cyo GufataIgikoresho cyo Gufata
Inkono y'icyuma cyasuweInkono y'icyuma cyasuwe
Termokupuli ifite igaragazaTermokupuli ifite igaragaza
4

Cool it slowly between magnesite blocks

Take the disc out and lay it between two magnesite blocks so it cools to room temperature over 1 hour. It comes out tough and even, close to its pressed shape.

Ibikoresho bikenewe:

Igikoresho cyo GufataIgikoresho cyo Gufata
Amatafari ya magnesiteAmatafari ya magnesite

Ibikoresho

1

Ibikoresho bikenewe

10

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