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Titanium: Titanium Tetrachloride Heated with Sodium in a Steel Bomb (Hunter, Thorpe 1913)
Sodium strips the chlorine from titanium tetrachloride inside a sealed steel bomb, leaving titanium metal in common salt.
Result: very pure titanium that looks like polished steel; hard and brittle cold, forgeable at low red heat, melting at 1800–1850 °C.
Source: Thorpe, Dictionary of Applied Chemistry vol. 5 (1913), p. 501, after Hunter (J. Amer. Chem. Soc. 1910, 32, 330). Thorpe does not say how the titanium is freed from the salt; ours follows Nagesh, Titanium Extraction Metallurgy (IntechOpen, 2023). Picture drawn by Youblob.
Hejuru
1 day
Amabwiriza
1
1
Charge the steel bomb
Charge the steel bomb
Weigh pure titanium tetrachloride and about half its weight of sodium into a steel bomb, and close it.
Ibikoresho by'iyi ntambwe:
Tetarakolorayide ya titane1 as requiredIbikoresho bikenewe:
Sodiyumu
Iminzani ya Digitale Nyayo
Ibombe y'icyuma2
2
Heat to low red heat
Heat to low red heat
Heat the bomb to a low red heat. Ours: a muffle furnace.
Ibikoresho bikenewe:
Ifuru ya muffle
Amakoro y'Icyombo Gishongesha3
3
Free the titanium
Free the titanium
Ours, after Nagesh, Titanium Extraction Metallurgy (IntechOpen, 2023): leach the reaction product with water, which dissolves the sodium chloride and the leftover sodium and leaves the titanium. Leftover sodium reacts violently with water and gives off hydrogen: add the product to the water a little at a time, away from flames. Ours: dry the metal in an oven.
Ibikoresho bikenewe:
Amazi
Igikombe cy'Ikirahure
Ifuru yo kumishahoIbikoresho
1- 1 as requiredUmwanya
Ibikoresho bikenewe
8- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
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