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Trisodium Phosphate: Phosphoric Acid, Soda, then Caustic Soda
Trisodium phosphate is the strongly alkaline sodium phosphate used to throw down cobalt violet. Thorpe (1913): soda added to phosphoric acid until alkaline gives disodium phosphate; excess caustic soda turns that into the trisodium salt, which crystallises in six-sided prisms. Caustic soda burns skin: gloves and goggles.
The picture: trisodium phosphate (Wikimedia Commons).
Utangiye
1 day
Amabwiriza
1
1
Phosphoric acid and soda
Phosphoric acid and soda
Goggles and gloves on. Dilute 100 g of 85 % phosphoric acid with water and stir in soda ash until the liquid is alkaline to litmus (about 92 g). Filter.
Ibikoresho by'iyi ntambwe:
Aside fosiforike (85 %)100 g
Karubonate ya Sodiyumu (ivu rya soda)92 gIbikoresho bikenewe:
Amazi
Igikombe cya Borosilikate
Akati k'Ikirahure ko Kuvanga
Urupapuro rwa litimusi
Umwenda w'ipamba woroheje wo kuyungurura
Umunzani w'ibiro
Amadarubindi yo Kwirinda Ibinyabutabire
Uturindantoki tw'ikawusu2
2
Add caustic soda
Add caustic soda
Dissolve about 40 g of caustic soda in a little water and add it to the disodium phosphate solution: a little more than the 35 g the equation needs.
Ibikoresho by'iyi ntambwe:
Umunyu w'umuriro (hydroxyde ya sodium)40 gIbikoresho bikenewe:
Amazi
Igikombe cya Borosilikate
Akati k'Ikirahure ko Kuvanga
Uturindantoki tw'ikawusu
Amadarubindi yo Kwirinda Ibinyabutabire3
3
Crystallise
Crystallise
Concentrate and let it crystallise; the free alkali stays in the mother liquor. Drain the six-sided prisms and keep them in a closed jar.
Ibikoresho bikenewe:
Isahani yo kumisha
Isahani y'umucanga
Icupa ry'Ikirahure Rifite UmufunikoIbikoresho
3- Umwanya
- Umwanya
- Umwanya
Ibikoresho bikenewe
11- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
- Umwanya
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