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Vanadium Trioxide: the Pentoxide Reduced with Carbon at Red Heat (Thorpe, 1913)
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4. Ugushyingo 2026DE
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Vanadium Trioxide: the Pentoxide Reduced with Carbon at Red Heat (Thorpe, 1913)

Vanadium trioxide, a black powder, made by heating vanadium pentoxide with carbon to a red heat. It is the oxide Gin reduced with ferro-silicon to make ferro-vanadium. Hot trioxide takes up oxygen quickly and turns back to the dioxide, so it is kept out of the air while hot. Source: T. E. Thorpe, Dictionary of Applied Chemistry vol. V (1913), p. 610. Picture: the book's text.
Hagati
Unknown

Amabwiriza

1

Mix pentoxide and carbon

Grind vanadium pentoxide with carbon. Proportions are not given.

Ibikoresho by'iyi ntambwe:

Ogiside ya vanadiyumuOgiside ya vanadiyumu1 igice
KaruboneKarubone1 igice

Ibikoresho bikenewe:

Isekuru n'UmuhiniIsekuru n'Umuhini
2

Reduce at red heat

Heat the mixture in a crucible to a red heat; the pentoxide is reduced to the trioxide, a black powder.

Ibikoresho bikenewe:

Icyombo cyo gushongeramoIcyombo cyo gushongeramo
Ifuru ya muffleIfuru ya muffle
3

Cool out of air

In air the trioxide oxidises slowly when cold and quickly when hot, forming the dioxide (Thorpe); so cool it with the crucible covered (our step).

Ibikoresho bikenewe:

Icyombo cyo gushongeramoIcyombo cyo gushongeramo

Ibikoresho

2

Ibikoresho bikenewe

3

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