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Metal Oxide Varistor: Pure Zinc Oxide at 800 °C, Bismuth Oxide Paste Fired at 800 °C (Masuyama 1972, Ex. 4)
Ed

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Ed

28. Ukwakira 2026FI
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Metal Oxide Varistor: Pure Zinc Oxide at 800 °C, Bismuth Oxide Paste Fired at 800 °C (Masuyama 1972, Ex. 4)

A varistor made the other way round: a disc of pure zinc oxide, sintered, with bismuth oxide fired into its faces from a paste instead of mixed in. Sintered at 800 °C and fired with the paste at 800 °C, the disc measured a C-value of 300 at 1 mA and a nonlinearity exponent n of 6.8. Masuyama found that firing on the bismuth oxide paste raises n a great deal over mixing it in. Source: T. Masuyama, M. Matsuoka and T. Nishi (Matsushita), US 3,663,458 (1972), Example 4. Unknown: what the silver paint is, and how strong the epoxy solution of the paste is. The spraying is ours, after US Army Corps of Engineers EM 1110-2-3401 (1999). The 10 g batch is our arithmetic. Picture: the patent's drawing.
Hejuru
2 days

Amabwiriza

1

Press pure zinc oxide at 340 kg/cm²

Press zinc oxide powder at 340 kg/cm². Example 4 gives no disc size; ours: discs 13 mm across and 2.5 mm thick in the mould of Example 1.

Ibikoresho by'iyi ntambwe:

Ifu ya oxide ya zinkiIfu ya oxide ya zinki1 as required

Ibikoresho bikenewe:

Umunzani w'ibiroUmunzani w'ibiro
Imashini ikanda ikoresha amaziImashini ikanda ikoresha amazi
Ifumbiro ryo gukanda disikiIfumbiro ryo gukanda disiki
Kalipe ya VernierKalipe ya Vernier
2

Sinter 1 hour at 800 °C and cool

Heat the pressed disc for 1 hour at 800 °C, then let it cool to room temperature.

Ibikoresho bikenewe:

Ifuru ya muffleIfuru ya muffle
3

Lap both faces

Lap both faces with silicon carbide abrasive. Example 4 gives no thickness.

Ibikoresho bikenewe:

Udukombe twa karubide ya silikoniUdukombe twa karubide ya silikoni
Kalipe ya VernierKalipe ya Vernier
4

Coat with bismuth oxide paste and fire at 800 °C

Coat both lapped faces with a paste of 50 % by weight bismuth oxide in a solution of epoxy resin in butyl alcohol, and fire it in air at 800 °C for 30 minutes. The bismuth oxide diffuses into the zinc oxide. Not given: how much paste, or the strength of the epoxy solution.

Ibikoresho by'iyi ntambwe:

Bisimuti okisideBisimuti okiside1 as required

Ibikoresho bikenewe:

Irembo rya epoxyIrembo rya epoxy
n-Butanoln-Butanol
Ifuru ya muffleIfuru ya muffle
5

Spray aluminium electrodes and attach leads

Spray a metallised film of aluminium on both faces. Attach a lead wire to each with conductive silver paint, as in Example 1. Ours, after US Army Corps of Engineers EM 1110-2-3401 (1999): wire-arc spray the aluminium from two 3.2 mm wires melted by an 18-40 V DC arc and atomised by compressed air, 15-20 cm from the disc and never at less than 45°, in at least two coats at right angles of 50-75 µm each. Unknown: the paint.

Ibikoresho by'iyi ntambwe:

Igice cya aluminiyumuIgice cya aluminiyumu1 as 3.2 mm spray wire
Irangi rya feza rinyuza amashanyaraziIrangi rya feza rinyuza amashanyarazi1 as required
Insinga y'UmuringaInsinga y'Umuringa2 ibice

Ibikoresho bikenewe:

Kalipe ya VernierKalipe ya Vernier
Imbunda yo kumisha ukoresheje urumuri rw'insingaImbunda yo kumisha ukoresheje urumuri rw'insinga
Igikandamiza umwuka cy'ingandaIgikandamiza umwuka cy'inganda

Ibikoresho

5

Ibikoresho bikenewe

10

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