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Barium Ferrite Disc Magnet: 1 mol BaCO3 to 3 mol Iron Oxide, 1330 °C (Went, Philips 1956, Ex. 2)
A barium ferrite with more iron oxide: 1 mol barium carbonate to 3 mol, made as in Example 1 and passed through a 1330 °C furnace in 20 minutes. Went's rod held 1,510 gauss with a coercive force of 2,080 oersted.
Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 2. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Advanced
2 days
Instructions
1
1
Weigh barium carbonate and iron oxide
Weigh barium carbonate and iron oxide
Weigh 201.1 g barium carbonate (1 mol) and 480.6 g ferric oxide (3 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.
Materials for this step:
Barium Carbonate (Witherite)201.1 g
Ferric Oxide480.6 gTools needed:
Balance Scale
Rubber Gloves
P100 Respirator2
2
Mill with alcohol 13.5 hours, dry and sieve
Mill with alcohol 13.5 hours, dry and sieve
Grind the mixture with alcohol in a ball mill for 13.5 hours, then dry it and sieve it.
Tools needed:
Iron Ball Mill
Ethanol - Lab Grade, 95%
Drying Oven
Sieve3
3
Knead with a binder and form
Knead with a binder and form
Mix 300 g of the powder with a binder such as polyvinyl alcohol (Went names it or nitrocellulose) into a kneadable mass. The patent extrudes rods about 3 mm across; ours: press discs at 1.5 tonnes per cm², as in its other examples. Dry them in air for about 24 hours.
Tools needed:
Polyvinyl Alcohol Powder
Hydraulic Press
Disc Pressing Die
Drying Oven4
4
Pass through a 1330 °C zone in 20 minutes
Pass through a 1330 °C zone in 20 minutes
Sinter in air at 1330 °C by passing the pieces through a 10 cm hot zone at 5 mm per minute: 20 minutes in the heat.
Tools needed:
Tube Furnace
Heat-Resistant Gloves5
5
Magnetise the discs
Magnetise the discs
The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.
Tools needed:
Electromagnet
CompassMaterials
2- 201.1 gPlaceholder
- 480.6 gPlaceholder
Tools Required
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