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Pressure Reactor: the Cast-Iron Autoclave with Bolted Cover (Thorpe, 1912)
The chemical works' autoclave, built on Papin's digester: a closed cast-iron vessel with a flanged cover bolted down on a lead washer, a pressure gauge, a safety valve and a thermometer tube. It heats liquids above their boiling points, often at 20 to 30 atmospheres, in a bath of hot oil or molten lead.
Variable: the material (cast iron, steel, copper, sheet iron) and lining (enamel, tin, lead, copper or zinc).
Source: Thorpe, Dictionary of Applied Chemistry, vol. I (1912), pp. 343-344. Unknown: sizes, wall thickness. Picture: Fig. 3 of the book.
Expert
Unknown
Instructions
1
1
Cast the body and cover
Cast the body and cover
Make the vessel of cast iron (or steel; occasionally copper, sheet iron or sheet steel), with a flange for the cover (Figs. 1-3). Cast-iron vessels are sometimes strapped with steel rings for safety. Not given: sizes and wall thickness.
Materials for this step:
Iron Castings2 body, cover
Mild Steel Flat Bar1 rings, optionalTools needed:
Unknown Dimensions2
2
Fit gauge, valve and thermometer tube
Fit gauge, valve and thermometer tube
Fit a pressure gauge, a safety valve and tubes for thermometers. If the charge would attack the iron, enamel the inside or line it with sheet tin, lead, copper or zinc soldered tight to the wall.
Materials for this step:
Pressure Gauge1 piece
Unknown Valve1 safety valve
Iron Tube1 thermometer tubeTools needed:
Spanner Set3
3
Close the cover
Close the cover
Close it with a screwed or flanged cover bearing on a lead washer, bolted down evenly.
Materials for this step:
Lead Sheet1 washer
Hex Bolt - Grade 8.81 flange bolts, number not givenTools needed:
Spanner Set4
4
Pressure-test and heat
Pressure-test and heat
Because it must hold 20 to 30 atmospheres, test it with hydraulic (water) pressure before use. In service, heat it by circulating hot oil or by standing it in a bath of molten lead.
Tools needed:
Hand Pressure Test Pump
Water
Molten Lead BathMaterials
7- 2 body, coverPlaceholder
- 1 rings, optionalPlaceholder
- 1 piecePlaceholder
- 1 safety valvePlaceholder
- 1 thermometer tubePlaceholder
- 1 washerPlaceholder
- 1 flange bolts, number not givenPlaceholder
Tools Required
5- Placeholder
- Placeholder
- Placeholder
- Placeholder
- Placeholder
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