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Sal Ammoniac Sublimed from Dung Soot, the Egyptian Way, Ure 1839
Sal ammoniac takes its name from the temple of Ammon in Egypt, where it was made from the soot of burned camel dung. Andrew Ure (1839): pack the soot into loam-coated glass globes over a furnace and heat them to a dull red; the salt rises and sets as a cake inside the top. Keep the necks clear or the globes can burst.
The picture: ammonium chloride crystals.
Advanced
A week
Instructions
1
1
Burn dung for soot
Burn dung for soot
Dry the dung by plastering it on a sunny wall. Burn it in the furnace with an iron sheet set as a hood over the smoke (ours), and scrape the soot off the sheet as it builds up.
Materials for this step:
Animal Dung100 kgTools needed:
Brick Furnace
Iron Sheet
Shovel
Dust Mask
Leather Work Gloves2
2
Coat and fill the globes
Coat and fill the globes
Coat glass flasks with a thick skin of loam (clay) and let it dry. Ram the soot in firmly, leaving two or three inches empty at the neck.
Tools needed:
Round-Bottom Flask
Clay
Wooden Mallet
Balance Scale
Dust Mask3
3
Sublime
Sublime
Set the globes in holes over the furnace flue and fire with dry dung, slowly at first, until they glow a dull red. The salt rises and cakes inside the top. Clear the necks often with an iron rod: a blocked neck can burst the globe.
Tools needed:
Brick Furnace
Animal Dung
Iron Rod
Leather Work Gloves
Safety Glasses4
4
Knock out the cake
Knock out the cake
When cold, the globes are usually cracked. Break the glass away from the white cake at the top with the back of a hatchet. Bruise the residue at the bottom and add it to the next charge. Store the salt in a jar.
Tools needed:
Axe
Glass Jar
Balance Scale
Leather Work Gloves
Safety Glasses5
5
Salt from your soot
Salt from your soot
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Materials
1- 100 kgPlaceholder
Tools Required
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