ART
BEAUTY & WELLNESS
CRAFT
CULTURE & HISTORY
ENTERTAINMENT
ENVIRONMENT
FOOD & DRINKS
REVERSE ENGINEERING
SCIENCES
SPORTS
TECHNOLOGY
WEARABLES
Tannic Acid: Powdered Galls Extracted with Ether (Pelouze, Pharmacopoeia Form)
Charlie

Created by

Charlie

20. October 2026DE
0
0
0
0
0

Tannic Acid: Powdered Galls Extracted with Ether (Pelouze, Pharmacopoeia Form)

Tannic acid (gallotannin) is richest in oak galls: the best, Aleppo galls, hold 50–60 %. This is Pelouze's method in the form the British and United States pharmacopoeias adopted, as given in Thorpe's Dictionary (1913): powdered galls are first kept in moist air, then extracted with ether. The liquid splits into two layers; the lower one is a strong solution of tannic acid that dries to a porous mass. No amounts are given. Ether is very flammable: no flame, fume hood. The picture: our diagram.
Intermediate
2 days

Instructions

1

Powder the galls and let them take up moisture

Grind oak galls finely. Leave the powder for some time in a moist atmosphere before extracting. Ours: a mortar, then a covered tray with a damp cloth.

Materials for this step:

Oak GallsOak Galls1 as required

Tools needed:

Stone Mortar and PestleStone Mortar and Pestle
Damp Cloth TrayDamp Cloth Tray
2

Extract with ether

Extract the powder with commercial ether. Ours: shake in a stoppered bottle in a fume hood, away from any flame.

Tools needed:

Diethyl EtherDiethyl Ether
Glass Bottles with StoppersGlass Bottles with Stoppers
Fume Hood (Ducted)Fume Hood (Ducted)
Chemical Splash GogglesChemical Splash Goggles
Rubber GlovesRubber Gloves
3

Separate the two layers

The extract separates into two layers. The upper is ether with gallic acid, wax and resins; the lower is a strong solution of tannic acid. Keep the lower layer. Ours: a separatory funnel.

Tools needed:

Separatory FunnelSeparatory Funnel
Fume Hood (Ducted)Fume Hood (Ducted)
4

Evaporate to a porous mass

Evaporate the lower layer; the tannic acid remains as a porous mass. Ours: an evaporating dish on a water bath, no open flame.

Tools needed:

Evaporating DishEvaporating Dish
Water BathWater Bath
Fume Hood (Ducted)Fume Hood (Ducted)

Materials

1
  • 1 as required
    Placeholder

Tools Required

10

This blueprint makes

CC0 Public Domain

This blueprint is released under CC0. You are free to copy, modify, distribute, and use this work for any purpose, without asking permission.

Support the Maker by purchasing products through their Blueprint where they earn a Maker Commission set by Vendors, or create a new iteration of this Blueprint and include it as a connection in your own Blueprint to share revenue.

Discussion

(0)

Log in to join the discussion

Loading comments...