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Barium Ferrite Disc Magnet: Barium Carbonate and Iron Oxide Sintered (Went, Philips 1956)
Charlie

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Charlie

28. uMfumfu 2026DE
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Barium Ferrite Disc Magnet: Barium Carbonate and Iron Oxide Sintered (Went, Philips 1956)

The dark grey ceramic magnet on fridges and in loudspeakers is barium ferrite. It is made from two cheap powders: one part barium carbonate to six of iron oxide, milled, fired, milled again, pressed and sintered. No cobalt or nickel is needed. This is Example 34 of the Philips patent. Fired 4 hours at 1100 °C, its rod held 1,375 gauss with a coercive force of 3,350 oersted. Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956). They pressed rods; the claim covers "a body of a desired shape", and the disc size is ours. The patent does not say how to magnetise it; our way is stated. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
Osezingeni eliphezulu
2 days

Imiyalelo

1

Weigh one part barium carbonate to six of iron oxide

Weigh 39.5 g of barium carbonate (0.2 mol) and 191.7 g of ferric oxide, Fe2O3 (1.2 mol). Barium carbonate is poisonous if swallowed: ours, gloves and a dust respirator.

Izinto zokwakha zalesi sinyathelo:

I-barium carbonate (i-witherite)I-barium carbonate (i-witherite)39.5 g
I-ferric oxideI-ferric oxide191.7 g

Amathuluzi adingekayo:

Isikali sesilinganisoIsikali sesilinganiso
Amagilavu erabhaAmagilavu erabha
Isivikelo Sokuphefumula i-P100Isivikelo Sokuphefumula i-P100
2

Mill with ethanol for 4 hours

Grind the mixture with ethanol in an iron ball mill for 4 hours. Let the ethanol evaporate, then dry the powder in a drying oven.

Amathuluzi adingekayo:

Umshini Wokugaya Ngamabhola EnsimbiUmshini Wokugaya Ngamabhola Ensimbi
I-ethanol - izinga lelabhorethri, 95 %I-ethanol - izinga lelabhorethri, 95 %
Ihhavini yokomisaIhhavini yokomisa
3

Presinter at 1000 °C for 4 hours

Fire the dry powder in air at 1000 °C for 4 hours (ours: in a lidded porcelain crucible in a muffle furnace). Let it cool.

Amathuluzi adingekayo:

Isithando se-muffleIsithando se-muffle
I-crucible enesivalo (i-porcelain)I-crucible enesivalo (i-porcelain)
Udlawu Lwesitsha SokuncibilikisaUdlawu Lwesitsha Sokuncibilikisa
Amagilavu Amelana NokushisaAmagilavu Amelana Nokushisa
4

Mill again for 4 hours

Grind the presintered product with ethanol in the ball mill for another 4 hours. Let the ethanol evaporate.

Amathuluzi adingekayo:

Umshini Wokugaya Ngamabhola EnsimbiUmshini Wokugaya Ngamabhola Ensimbi
I-ethanol - izinga lelabhorethri, 95 %I-ethanol - izinga lelabhorethri, 95 %
Ihhavini yokomisaIhhavini yokomisa
Isivikelo Sokuphefumula i-P100Isivikelo Sokuphefumula i-P100
5

Press discs at 1.5 tons per cm²

Press the powder at 1.5 tons/cm². The patent pressed rods; we press discs. Ours: a die 20 mm across, so about 4.7 tonnes on the punch (our arithmetic: 1.5 × 3.14 cm²).

Amathuluzi adingekayo:

Umshini wokucindezela we-hydraulicUmshini wokucindezela we-hydraulic
Isikhunta sokucindezela idiskiIsikhunta sokucindezela idiski
6

Sinter for 4 hours

Sinter the discs for 4 hours in oxygen or in air. The patent's results: at 1100 °C, 1,375 gauss and 3,350 oersted; at 1200 °C, 1,400 and 3,100; at 1300 °C, 1,850 and 1,780. Hotter gives a stronger but less stubborn magnet.

Amathuluzi adingekayo:

Isithando se-muffleIsithando se-muffle
Udlawu Lwesitsha SokuncibilikisaUdlawu Lwesitsha Sokuncibilikisa
Amagilavu Amelana NokushisaAmagilavu Amelana Nokushisa
7

Magnetise the discs

The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.

Amathuluzi adingekayo:

I-electromagnetI-electromagnet
IkhompasiIkhompasi

Izinto

2

Amathuluzi Adingekayo

14

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