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Tannic Acid: Chinese Galls Extracted with Warm Water, Shaken with Ether and Dried on Tin Sheets
This is the large-scale way to make commercial tannin, as Thorpe's Dictionary (1913) gives it. Chinese galls from sumach hold as much as 70 % tannin; the best oak galls, from Aleppo, 50–60 %. The powder is extracted with warm water, and the extract is shaken with ether. After several days the ether layer on top is taken off; the tannin stays in the lower layer, which is dried on hot tin sheets until it puffs up. The product still holds some gallic acid, wax and glucose. Ether is very flammable: no flame.
The picture: our diagram.
Ophakathi
1 week
Imiyalelo
1
1
Extract the powdered galls with warm water
Extract the powdered galls with warm water
Powder Chinese galls finely. Stir with enough water at 50–60 °C to make a strong extract. Filter it clear.
Izinto zokwakha zalesi sinyathelo:
Ama-Gall AseShayina1 as requiredAmathuluzi adingekayo:
Amanzi
Isigqulo Nomgqulo Wetshe
Isigovuzi
Ibhavu Lamanzi
Ithemomitha Yaselabhorethri
Iphepha Lokuhluza
Ifanela Lengilazi Elinomlomo2
2
Shake with a quarter volume of ether
Shake with a quarter volume of ether
Add ether, one quarter of the extract's volume, and agitate until it forms an emulsion. Let it stand for several days.
Amathuluzi adingekayo:
I-diethyl ether
Isitheleli Sokuhlukanisa
Ikhabethe lomusi (elinepayipi)
Izibuko Zokuchitheka Kwamakhemikhali
Amagilavu erabha3
3
Take off the ether layer and recover the ether
Take off the ether layer and recover the ether
Remove the upper ether layer. Run the lower layer, which holds all the tannin, into a still and distil off the ether in it to recover it. No flame near the ether.
Amathuluzi adingekayo:
Isitheleli Sokuhlukanisa
I-alembic yethusi
Ikhabethe lomusi (elinepayipi)4
4
Dry on tin sheets over a steam coil
Dry on tin sheets over a steam coil
Let the syrupy liquid cool, spread it on tin sheets and heat them with a steam coil. The tannin quickly puffs up and dries.
Amathuluzi adingekayo:
Ipuleti lethini
Ikhoyili Yesitimu
Ibhayela lesitimu
Amagilavu erabhaIzinto
1- 1 as requiredIsibambeli
Amathuluzi Adingekayo
16- Isibambeli
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