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Tannic Acid: Powdered Galls Extracted with Ether and Alcohol (75:25)
Pelouze's way of getting tannic acid from galls uses ether; Thorpe's Dictionary (1913) notes that a mixture of 75 % ether and 25 % alcohol can be used in its place. The extract separates into two layers, and the lower one, a strong tannic acid solution, dries to a porous mass. No amounts are given. Ether is very flammable: no flame, fume hood.
The picture: our diagram.
Ophakathi
1 day
Imiyalelo
1
1
Powder the galls
Powder the galls
Grind oak galls finely. Ours: a mortar.
Izinto zokwakha zalesi sinyathelo:
Ama-gall omuthi wom-oak1 as requiredAmathuluzi adingekayo:
Isigqulo Nomgqulo Wetshe2
2
Extract with 75 % ether, 25 % alcohol
Extract with 75 % ether, 25 % alcohol
Mix 75 parts commercial ether with 25 parts alcohol and extract the powder with it. Ours: shake in a stoppered bottle in a fume hood, away from any flame.
Amathuluzi adingekayo:
I-diethyl ether
I-ethanol - izinga lelabhorethri, 95 %
Isilinda esinezilinganiso
Amabhodlela engilazi anezivimbo
Ikhabethe lomusi (elinepayipi)
Izibuko Zokuchitheka Kwamakhemikhali
Amagilavu erabha3
3
Keep the lower layer and evaporate it
Keep the lower layer and evaporate it
The extract separates into two layers: gallic acid, wax and resins in the upper, a strong tannic acid solution in the lower. Evaporate the lower layer to a porous mass. Ours: separatory funnel, evaporating dish on a water bath.
Amathuluzi adingekayo:
Isitheleli Sokuhlukanisa
Ipuleti Lokuhwamuka
Ibhavu Lamanzi
Ikhabethe lomusi (elinepayipi)Izinto
1- 1 as requiredIsibambeli
Amathuluzi Adingekayo
11- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
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