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Trisodium Phosphate: Phosphoric Acid, Soda, then Caustic Soda
Trisodium phosphate is the strongly alkaline sodium phosphate used to throw down cobalt violet. Thorpe (1913): soda added to phosphoric acid until alkaline gives disodium phosphate; excess caustic soda turns that into the trisodium salt, which crystallises in six-sided prisms. Caustic soda burns skin: gloves and goggles.
The picture: trisodium phosphate (Wikimedia Commons).
Oqalayo
1 day
Imiyalelo
1
1
Phosphoric acid and soda
Phosphoric acid and soda
Goggles and gloves on. Dilute 100 g of 85 % phosphoric acid with water and stir in soda ash until the liquid is alkaline to litmus (about 92 g). Filter.
Izinto zokwakha zalesi sinyathelo:
I-asidi ye-phosphoric (85 %)100 g
I-Sodium Carbonate (umlotha we-soda)92 gAmathuluzi adingekayo:
Amanzi
Ibhikha Le-borosilicate
Induku Yengilazi Yokugovuza
Iphepha le-litmus
Indwangu yokuhluza kakotini encane
Isikali sesilinganiso
Izibuko Zokuchitheka Kwamakhemikhali
Amagilavu erabha2
2
Add caustic soda
Add caustic soda
Dissolve about 40 g of caustic soda in a little water and add it to the disodium phosphate solution: a little more than the 35 g the equation needs.
Izinto zokwakha zalesi sinyathelo:
I-caustic soda (i-sodium hydroxide)40 gAmathuluzi adingekayo:
Amanzi
Ibhikha Le-borosilicate
Induku Yengilazi Yokugovuza
Amagilavu erabha
Izibuko Zokuchitheka Kwamakhemikhali3
3
Crystallise
Crystallise
Concentrate and let it crystallise; the free alkali stays in the mother liquor. Drain the six-sided prisms and keep them in a closed jar.
Amathuluzi adingekayo:
Ipuleti Lokuhwamuka
Ibhavu lesihlabathi
Ijeke Lengilazi ElinesivaloIzinto
3- Isibambeli
- Isibambeli
- Isibambeli
Amathuluzi Adingekayo
11- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
- Isibambeli
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