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Barium Ferrite Disc Magnet: 0.5 mol BaCO3 to 3.5 mol Iron Oxide, 10 Minutes at 1330 °C (Went, Philips 1956, Ex. 4)
A barium ferrite with much more iron oxide: 0.5 mol barium carbonate to 3.5 mol, milled 15.5 hours, bound, formed and sintered 10 minutes at 1330 °C. Went's rod held 2,040 gauss with a coercive force of 2,380 oersted.
Source: J. J. Went, G. W. van Oosterhout and E. W. Gorter (Philips), US 2,762,777 (1956), Example 4. They sintered rods; discs and the magnetising are ours. Picture: ferrite magnets, Omegatron, Wikimedia Commons, CC BY-SA 3.0.
高级
2 days
说明
1
1
Weigh barium carbonate and iron oxide
Weigh barium carbonate and iron oxide
Weigh 99.2 g barium carbonate (0.5 mol) and 564.8 g ferric oxide (3.5 mol). Barium carbonate is poisonous if swallowed: gloves and a dust respirator.
此步骤所需材料：
碳酸钡（毒重石）99.2 克
氧化铁564.8 克所需工具：
等臂天平
橡胶手套
P100 防毒面具2
2
Mill with alcohol 15.5 hours, dry and sieve
Mill with alcohol 15.5 hours, dry and sieve
Grind the mixture with alcohol in a ball mill for 15.5 hours, then dry it and sieve it.
所需工具：
铁球磨机
乙醇——实验级，95 %
干燥炉
粗筛3
3
Knead with a binder and form
Knead with a binder and form
Mix 300 g of the powder with a binder such as polyvinyl alcohol (Went names it or nitrocellulose) into a kneadable mass. The patent extrudes rods about 3 mm across; ours: press discs at 1.5 tonnes per cm², as in its other examples. Dry them in air for about 24 hours.
所需工具：
聚乙烯醇粉末
液压机
圆片压模干燥炉4
4
Sinter in air at 1330 °C for 10 minutes
Sinter in air at 1330 °C for 10 minutes
Sinter the pieces in air at 1330 °C for 10 minutes. The patent gives no zone length or speed for this example.
所需工具：
管式炉
耐热手套5
5
Magnetise the discs
Magnetise the discs
The patent gives no magnetising method. Ours: lay a disc with its faces against the poles of a strong electromagnet, switch the current on, then off. Find which face is north with a compass.
所需工具：
电磁铁
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